Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C23H22BNO2 |
| M r | 355.22 |
| Crystal system, space group | Orthorhombic, P c a21 |
| Temperature (K) | 100 |
| a, b, c (Å) | 17.8540 (11), 11.5361 (6), 18.5366 (12) |
| V (Å3) | 3817.9 (4) |
| Z | 8 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.08 |
| Crystal size (mm) | 0.38 × 0.2 × 0.07 |
| Data collection | |
| Diffractometer | Bruker–Nonius Kappa APEXII |
| Absorption correction | Multi-scan (SADABS; Bruker, 2015 ▸) |
| T min, T max | 0.703, 0.733 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 60829, 8781, 7379 |
| R int | 0.047 |
| (sin θ/λ)max (Å−1) | 0.652 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.039, 0.086, 1.03 |
| No. of reflections | 8781 |
| No. of parameters | 491 |
| No. of restraints | 1 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.25, −0.24 |