Refinement on F2	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.065	Hydrogen site location: mixed
wR(F2) = 0.143	H atoms treated by a mixture of independent and constrained refinement
S = 1.07	w = 1/[σ2(Fo2) + (0.0001P)2 + 29.7569P] where P = (Fo2 + 2Fc2)/3
28700 reflections	(Δ/σ)max = 0.001
1153 parameters	Δρmax = 2.44 e Å−3
1810 restraints	Δρmin = −2.18 e Å−3