Bruker SMART APEX CCD diffractometer | 6598 independent reflections |
Radiation source: fine-focus sealed tube | 5337 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.040 |
Detector resolution: 8.3333 pixels mm-1 | θmax = 29.3°, θmin = 2.0° |
φ and ω scans | h = −8→8 |
Absorption correction: multi-scan (SADABS; Krause et al., 2015) | k = −13→13 |
Tmin = 0.23, Tmax = 0.56 | l = −29→29 |
24139 measured reflections |