| Rigaku R-AXIS RAPID diffractometer | 3589 reflections with I > 2σ(I) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.025 |
| ω scans | θmax = 27.5°, θmin = 3.3° |
| Absorption correction: multi-scan (ABSCOR; Rigaku, 1995) | h = −30→30 |
| Tmin = 0.684, Tmax = 0.941 | k = −10→10 |
| 15965 measured reflections | l = −21→21 |
| 3768 independent reflections |
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