| Bruker APEXII CCD diffractometer | 2477 reflections with I≥ 2u(I) |
| φ and ω scans | Rint = 0.139 |
| Absorption correction: multi-scan (SADABS; Bruker, 2016) | θmax = 25.1°, θmin = 3.0° |
| Tmin = 0.368, Tmax = 0.746 | h = −14→14 |
| 31593 measured reflections | k = −11→11 |
| 3668 independent reflections | l = −29→29 |