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(a) Temperature-dependent cyclic voltammograms of [Bu4N][LCuOH] (1.0 mM) + Fc* (0.5 mM) in CH2Cl2, at 1.0 M (blue) and 0.2 M (red) electrolyte (TBAP = [NBu4][PF6]). 0.2 M [Bu4N][PF6] as electrolyte; sweep rate = 50 mV s−1. (b) Plot of ΔE1/2 vs T, where ΔE1/2 = E1/2(Cu) − E1/2(Fc*).
