Table 3.
Recoveries and matrix effects of 5 compounds (n = 3).
Compounds | Concentration (ng/mL) | Recovery | Matrix effect | ||
---|---|---|---|---|---|
Mean ± SD (%) | RSD (%) | Mean ± SD (%) | RSD (%) | ||
Geniposidic acid | 10 | 96.7 ± 4.8 | 4.96 | 114 ± 10 | 8.77 |
30 | 110 ± 13 | 11.82 | 103 ± 10 | 9.71 | |
300 | 111 ± 6 | 5.41 | 110 ± 4 | 3.64 | |
3000 | 97.8 ± 4.1 | 4.19 | 115 ± 2 | 1.74 | |
| |||||
Genipin-1-β-gentiobioside | 10 | 97.2 ± 5.5 | 5.66 | 92.5 ± 7.5 | 8.11 |
30 | 94.7 ± 2.1 | 2.22 | 114 ± 4 | 3.51 | |
300 | 100 ± 12 | 12.01 | 88.6 ± 5.7 | 6.43 | |
3000 | 94.8 ± 4.1 | 4.32 | 93.9 ± 4.7 | 5.01 | |
| |||||
Geniposide | 10 | 97.4 ± 9.4 | 9.65 | 97.3 ± 11.5 | 11.82 |
30 | 110 ± 4 | 3.64 | 96.4 ± 3.7 | 3.84 | |
300 | 84.3 ± 4.0 | 4.74 | 106 ± 6.6 | 6.23 | |
3000 | 104 ± 3 | 2.88 | 111 ± 6 | 5.41 | |
| |||||
Genipin | 10 | 81.2 ± 11.0 | 13.55 | 106 ± 9 | 8.49 |
30 | 81.0 ± 7.4 | 9.14 | 115 ± 2 | 1.74 | |
300 | 111 ± 11 | 9.91 | 104 ± 9 | 8.65 | |
3000 | 114 ± 5 | 4.39 | 92.9 ± 5.2 | 5.60 | |
| |||||
Crocetin | 10 | 103 ± 8. | 7.77 | 89.1 ± 4.2 | 4.71 |
30 | 95.8 ± 10.0 | 10.44 | 94.3 ± 6.8 | 7.21 | |
300 | 99.2 ± 13.4 | 13.51 | 98.0 ± 13.2 | 13.47 | |
3000 | 98.5 ± 10.0 | 10.15 | 98.3 ± 5.4 | 5.49 |