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. 2020 May 1;25(9):2128. doi: 10.3390/molecules25092128

Scheme 4.

Scheme 4

Reactions of PhMgBr with substituted thiochromones. a. All the reactions were performed using 1.5 equiv of PhMgBr in the presence of 2.0 equiv of TMSCI unless noted otherwise. b. PhMgBr were commercially available. c. Yields are based on isolated products by column chromatography.