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. 2020 May 12;5(20):11342–11351. doi: 10.1021/acsomega.0c00303

Table 6. Combinations of Compounds Tested and Their Reaction Temperatures and Durations.

run U:Fa (molar ratio) F:NH3b (molar ratio) reaction temperature (°C) reaction time (h)
1 0.75 1.33 60 1.5
2 1.25 1.33 60 1.5
3 0.75 2.67 60 1.5
4 1.25 2.67 60 1.5
5 0.75 1.33 100 1.5
6 1.25 1.33 100 1.5
7 0.75 2.67 100 1.5
8 1.25 2.67 100 1.5
9 0.75 1.33 60 3.5
10 1.25 1.33 60 3.5
11 0.75 2.67 60 3.5
12 1.25 2.67 60 3.5
13 0.75 1.33 100 3.5
14 1.25 1.33 100 3.5
15 0.75 2.67 100 3.5
16 1.25 2.67 100 3.5
17 0.5 2 80 2.5
18 1.5 2 80 2.5
19 1 0.66 80 2.5
20 1 3.34 80 2.5
21 1 2 40 2.5
22 1 2 120 2.5
23 1 2 80 0.5
24 1 2 80 4.5
25 1 2 80 2.5
26 1 2 80 2.5
27 1 2 80 2.5
28 1 2 80 2.5
29 1 2 80 2.5
30 1 2 80 2.5
a

Urea/formaldehyde ratio.

b

Formaldehyde/amine ratio.