Table 6. Combinations of Compounds Tested and Their Reaction Temperatures and Durations.
run | U:Fa (molar ratio) | F:NH3b (molar ratio) | reaction temperature (°C) | reaction time (h) |
---|---|---|---|---|
1 | 0.75 | 1.33 | 60 | 1.5 |
2 | 1.25 | 1.33 | 60 | 1.5 |
3 | 0.75 | 2.67 | 60 | 1.5 |
4 | 1.25 | 2.67 | 60 | 1.5 |
5 | 0.75 | 1.33 | 100 | 1.5 |
6 | 1.25 | 1.33 | 100 | 1.5 |
7 | 0.75 | 2.67 | 100 | 1.5 |
8 | 1.25 | 2.67 | 100 | 1.5 |
9 | 0.75 | 1.33 | 60 | 3.5 |
10 | 1.25 | 1.33 | 60 | 3.5 |
11 | 0.75 | 2.67 | 60 | 3.5 |
12 | 1.25 | 2.67 | 60 | 3.5 |
13 | 0.75 | 1.33 | 100 | 3.5 |
14 | 1.25 | 1.33 | 100 | 3.5 |
15 | 0.75 | 2.67 | 100 | 3.5 |
16 | 1.25 | 2.67 | 100 | 3.5 |
17 | 0.5 | 2 | 80 | 2.5 |
18 | 1.5 | 2 | 80 | 2.5 |
19 | 1 | 0.66 | 80 | 2.5 |
20 | 1 | 3.34 | 80 | 2.5 |
21 | 1 | 2 | 40 | 2.5 |
22 | 1 | 2 | 120 | 2.5 |
23 | 1 | 2 | 80 | 0.5 |
24 | 1 | 2 | 80 | 4.5 |
25 | 1 | 2 | 80 | 2.5 |
26 | 1 | 2 | 80 | 2.5 |
27 | 1 | 2 | 80 | 2.5 |
28 | 1 | 2 | 80 | 2.5 |
29 | 1 | 2 | 80 | 2.5 |
30 | 1 | 2 | 80 | 2.5 |
Urea/formaldehyde ratio.
Formaldehyde/amine ratio.