Figure 2.
(a) Geometric illustration of the energy-dispersive setup. The ~4 mrad cone angle of the x-ray source together with a Laue crystal results in an energy gradient across the detector. (b) The source spectrum was tuned to 26 keV configuration for Ag measurement (measured with an energy-dispersive detector, KETEK AXAS-D, KETEK GmbH, Munich, Germany). The inset shows a zoom-in of the spectrum. The colored regions indicate the energy ranges that can be covered by Si(311) and Si(111) diffracted beams, corresponding to XAS images in Fig. 3.