PDB Accession Code	6w4h	6w61
Crystallization Conditions
Screen conditions	0.2M Calcium acetate, 0.1M HEPES pH 7.5, 18% (w/v) PEG8000	0.1 M sodium citrate, pH 5.6, 10% (w/v) PEG4000, 10%(w/v) isopropanol
Protein concentration (mg/ml)	5.3	16.7
Data Collection
Space group	P3121	P3121
Unit cell parameters (Å; °)	a = 167.7, b = 167.7, c = 51.9; α = β=90.0, γ = 120.0	a = 168.6, b = 168.6, c = 52.0; α = β =90.0, γ = 120.0
Resolution range (Å)	30.00 – 1.80 (1.83 - 1.80)	50.00 - 2.00 (2.04 - 2.00)
No. of reflections	77,886 (3,873)	57,010 (2,781)
Rmerge (%)	6.0 (76.5)	13.9 (233.0)
Completeness (%)	100.0 (100.0)	100.0 (100.0)
<I/σ(I)>	29.3 (2.6)	37.1 (1.0)
Multiplicity	7.3 (6.8)	6.2 (6.3)
Wilson B factor	25.4	49.0
Structure Determination
MR initial model (PDB ID)	3r24	6w4h
Refinement
Resolution range (Å)	29.76 - 1.80 (1.85 - 1.80)	42.33 - 2.00 (2.04 - 2.00)
Completeness (%)	100.0 (100.0)	99.7 (96.3)
No. of reflections	73,752 (5,432)	56,859 (2,522)
Rwork/Rfree, (%)	14.9/16.3 (22.9/23.9)	17.2/19.3 (30.4/32.3)
Protein chains/atoms	2/3,201	2/3,390
Ligand/Solvent atoms	65/442	6/141
Mean temperature factor (Å2)	31.5	41.0
Coordinate Deviations
R.m.s.d. bonds (Å)	0.004	0.002
R.m.s.d. angles (°)	1.183	0.473
Ramachandran plot
Favored (%)	97.0	96.8
Allowed (%)	3.0	3.2
Outside allowed (%)	0.0	0.0