Table 5. Isolated Yield of Condensation Product Using MgO Calcined at Different Temperaturesa.
entry | MgO particles | isolated yield (%) |
---|---|---|
1 | MgOS_400 | 87 |
2 | MgOS_600 | 76 |
3 | MgOS_800 | 67 |
4 | MgOA_800 | 10 |
Reaction conditions: benzaldehyde, 4 mmol; malononitrile, 6 mmol; MgO, 20 mg; oil phase, 3 mL; water, 3 mL; room temperature, 30 min.