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. 2020 May 17;5(21):12148–12153. doi: 10.1021/acsomega.0c00467

Table 1. 13C NMR (150 MHz) Spectroscopic Data for Compounds 1–5 in CD3ODa.

no. 1 2 3 4 5
1 210.7 213.0 206.2 205.8 206.9
2 39.9 43.2 127.6 127.6 128.7
3 77.6 69.3 142.7 142.3 144.5
4 73.7 78.4 76.0 35.2 36.6
5 63.5 64.7 73.4 76.5 78.3
6 58.6 60.7 73.4 73.1 75.4
7 24.1 27.1 27.8 27.8 28.8
8 35.0 34.0 35.7 33.5 34.7
9 38.0 41.8 35.3 34.4 33.2
10 52.1 52.0 51.6 51.6 55.5
11 20.2 21.8 23.0 22.1 22.5
12 32.9 37.5 32.3 32.8 36.7
13 50.3 54.4 44.2 43.2 54.0
14 81.3 82.2 81.1 82.0 79.4
15 83.4 88.4 82.6 83.4 211.5
16 121.1 39.9 32.9 33.3 129.8
17 161.6 86.7 52.2 51.9 189.4
18 14.8 21.2 14.1 15.0 19.9
19 13.3 15.0 14.0 13.0 14.4
20 35.0 83.7 78.6 79.4 38.2
21 16.8 15.0 10.9 19.8 17.6
22 79.9 80.6 78.6 77.0 81.0
23 27.1 33.9 32.3 28.6 34.5
24 152.8 153.9 152.8 153.1 152.5
25 120.8 121.7 120.2 120.2 122.2
26 167.7 169.6 168.4 168.8 168.7
27 10.5 9.2 8.6 10.3 12.4
28 60.2 21.4 19.1 18.5 20.4
CH3CO-1′ 170.1 171.4 170.1 171.0  
CH3CO-2′ 19.9 20.5 19.9 19.1  
OMe 52.1        
a

Chemical shifts are in ppm, and the assignments were based on HSQC, HMBC, and NOSEY spectra.