| O1—C5 | 1.2098 (19) | C3—H3 | 0.9800 |
| O2—C5 | 1.345 (2) | C4—H4A | 0.9700 |
| O2—C6 | 1.446 (2) | C4—H4B | 0.9700 |
| O3—C8 | 1.1961 (19) | C6—C7 | 1.484 (3) |
| O4—C8 | 1.3312 (19) | C6—H6A | 0.9700 |
| O4—C9 | 1.445 (2) | C6—H6B | 0.9700 |
| O5—C10 | 1.195 (2) | C7—H7A | 0.9600 |
| O6—C10 | 1.3499 (19) | C7—H7B | 0.9600 |
| O6—C2 | 1.4385 (18) | C7—H7C | 0.9600 |
| O7—C12 | 1.195 (2) | C9—H9A | 0.9600 |
| O8—C12 | 1.348 (2) | C9—H9B | 0.9600 |
| O8—C3 | 1.4496 (19) | C9—H9C | 0.9600 |
| N1—C5 | 1.351 (2) | C10—C11 | 1.483 (3) |
| N1—C1 | 1.4518 (19) | C11—H11A | 0.9600 |
| N1—C4 | 1.464 (2) | C11—H11B | 0.9600 |
| C1—C8 | 1.524 (2) | C11—H11C | 0.9600 |
| C1—C2 | 1.528 (2) | C12—C13 | 1.496 (3) |
| C1—H1 | 0.9800 | C13—H13A | 0.9600 |
| C2—C3 | 1.521 (2) | C13—H13B | 0.9600 |
| C2—H2 | 0.9800 | C13—H13C | 0.9600 |
| C3—C4 | 1.523 (2) | ||
| C5—O2—C6 | 115.92 (14) | O2—C6—H6B | 110.4 |
| C8—O4—C9 | 115.73 (15) | C7—C6—H6B | 110.4 |
| C10—O6—C2 | 116.20 (12) | H6A—C6—H6B | 108.6 |
| C12—O8—C3 | 118.19 (13) | C6—C7—H7A | 109.5 |
| C5—N1—C1 | 121.34 (13) | C6—C7—H7B | 109.5 |
| C5—N1—C4 | 125.77 (13) | H7A—C7—H7B | 109.5 |
| C1—N1—C4 | 112.89 (12) | C6—C7—H7C | 109.5 |
| N1—C1—C8 | 111.47 (13) | H7A—C7—H7C | 109.5 |
| N1—C1—C2 | 102.32 (12) | H7B—C7—H7C | 109.5 |
| C8—C1—C2 | 113.23 (13) | O3—C8—O4 | 124.90 (16) |
| N1—C1—H1 | 109.9 | O3—C8—C1 | 125.34 (15) |
| C8—C1—H1 | 109.9 | O4—C8—C1 | 109.73 (13) |
| C2—C1—H1 | 109.9 | O4—C9—H9A | 109.5 |
| O6—C2—C3 | 108.78 (12) | O4—C9—H9B | 109.5 |
| O6—C2—C1 | 106.68 (12) | H9A—C9—H9B | 109.5 |
| C3—C2—C1 | 103.23 (12) | O4—C9—H9C | 109.5 |
| O6—C2—H2 | 112.5 | H9A—C9—H9C | 109.5 |
| C3—C2—H2 | 112.5 | H9B—C9—H9C | 109.5 |
| C1—C2—H2 | 112.5 | O5—C10—O6 | 122.72 (16) |
| O8—C3—C2 | 102.26 (11) | O5—C10—C11 | 125.62 (16) |
| O8—C3—C4 | 111.80 (12) | O6—C10—C11 | 111.66 (16) |
| C2—C3—C4 | 103.54 (13) | C10—C11—H11A | 109.5 |
| O8—C3—H3 | 112.8 | C10—C11—H11B | 109.5 |
| C2—C3—H3 | 112.8 | H11A—C11—H11B | 109.5 |
| C4—C3—H3 | 112.8 | C10—C11—H11C | 109.5 |
| N1—C4—C3 | 103.35 (12) | H11A—C11—H11C | 109.5 |
| N1—C4—H4A | 111.1 | H11B—C11—H11C | 109.5 |
| C3—C4—H4A | 111.1 | O7—C12—O8 | 122.72 (18) |
| N1—C4—H4B | 111.1 | O7—C12—C13 | 126.78 (18) |
| C3—C4—H4B | 111.1 | O8—C12—C13 | 110.46 (16) |
| H4A—C4—H4B | 109.1 | C12—C13—H13A | 109.5 |
| O1—C5—O2 | 125.04 (15) | C12—C13—H13B | 109.5 |
| O1—C5—N1 | 124.93 (15) | H13A—C13—H13B | 109.5 |
| O2—C5—N1 | 110.02 (14) | C12—C13—H13C | 109.5 |
| O2—C6—C7 | 106.76 (17) | H13A—C13—H13C | 109.5 |
| O2—C6—H6A | 110.4 | H13B—C13—H13C | 109.5 |
| C7—C6—H6A | 110.4 | ||
| C5—N1—C1—C8 | 76.02 (19) | C2—C3—C4—N1 | −27.36 (15) |
| C4—N1—C1—C8 | −103.88 (15) | C6—O2—C5—O1 | −0.3 (3) |
| C5—N1—C1—C2 | −162.67 (14) | C6—O2—C5—N1 | −179.62 (15) |
| C4—N1—C1—C2 | 17.43 (18) | C1—N1—C5—O1 | 2.0 (3) |
| C10—O6—C2—C3 | −96.72 (15) | C4—N1—C5—O1 | −178.13 (17) |
| C10—O6—C2—C1 | 152.54 (13) | C1—N1—C5—O2 | −178.67 (14) |
| N1—C1—C2—O6 | 80.73 (14) | C4—N1—C5—O2 | 1.2 (2) |
| C8—C1—C2—O6 | −159.17 (12) | C5—O2—C6—C7 | 178.98 (17) |
| N1—C1—C2—C3 | −33.83 (15) | C9—O4—C8—O3 | −6.4 (3) |
| C8—C1—C2—C3 | 86.27 (14) | C9—O4—C8—C1 | 171.57 (15) |
| C12—O8—C3—C2 | −176.59 (13) | N1—C1—C8—O3 | −8.7 (2) |
| C12—O8—C3—C4 | 73.23 (17) | C2—C1—C8—O3 | −123.40 (18) |
| O6—C2—C3—O8 | 168.91 (11) | N1—C1—C8—O4 | 173.33 (13) |
| C1—C2—C3—O8 | −78.04 (13) | C2—C1—C8—O4 | 58.60 (17) |
| O6—C2—C3—C4 | −74.78 (14) | C2—O6—C10—O5 | 3.0 (2) |
| C1—C2—C3—C4 | 38.26 (15) | C2—O6—C10—C11 | −176.72 (15) |
| C5—N1—C4—C3 | −173.74 (15) | C3—O8—C12—O7 | 0.4 (2) |
| C1—N1—C4—C3 | 6.15 (18) | C3—O8—C12—C13 | −177.58 (14) |
| O8—C3—C4—N1 | 82.01 (15) |