Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C14H16 |
| M r | 184.27 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 213 |
| a, b, c (Å) | 11.3214 (9), 6.7426 (6), 14.9478 (12) |
| β (°) | 107.234 (9) |
| V (Å3) | 1089.82 (16) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.06 |
| Crystal size (mm) | 0.26 × 0.23 × 0.20 |
| Data collection | |
| Diffractometer | Stoe IPDS |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 9458, 2593, 1885 |
| R int | 0.039 |
| (sin θ/λ)max (Å−1) | 0.661 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.044, 0.124, 0.99 |
| No. of reflections | 2593 |
| No. of parameters | 191 |
| H-atom treatment | All H-atom parameters refined |
| Δρmax, Δρmin (e Å−3) | 0.29, −0.17 |