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. 2020 May 22;76(Pt 6):896–899. doi: 10.1107/S2056989020006441
XtaLAB Synergy, Single source at offset/far, HyPix3000 diffractometer 4798 independent reflections
Radiation source: micro-focus sealed X-ray tube, PhotonJet (Mo) X-ray Source 4437 reflections with I > 2σ(I)
Mirror monochromator Rint = 0.036
Detector resolution: 10.0000 pixels mm-1 θmax = 27.4°, θmin = 1.9°
ω scans h = −9→9
Absorption correction: empirical (using intensity measurements) (CrysAlisPro; Rigaku OD, 2019) k = −14→14
Tmin = 0.735, Tmax = 1.000 l = −32→32
54562 measured reflections