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. 2020 May 5;76(Pt 6):798–802. doi: 10.1107/S2056989020005939
C1A—N1A 1.4597 (17) C6B—C7B 1.378 (2)
C1A—N2A 1.4646 (19) C6B—H6B 0.9300
C1A—C2A 1.5079 (17) C9A—C18A 1.3728 (18)
C1A—H1A 0.9800 C9A—C10A 1.4181 (19)
N1A—C9A 1.3944 (17) C7B—H7B 0.9300
N1A—H1N1 0.873 (19) C10A—C11A 1.4154 (17)
O1A—C3A 1.3693 (18) C10A—C15A 1.4189 (18)
O1A—H1OA 0.86 (2) C9B—C18B 1.372 (2)
C2A—C7A 1.388 (2) C9B—C10B 1.416 (2)
C2A—C3A 1.3923 (19) C11A—C12A 1.368 (2)
N2A—C11A 1.4081 (17) C10B—C11B 1.418 (2)
N2A—H1NA 0.870 (19) C10B—C15B 1.426 (2)
O1B—C3B 1.3616 (17) C12A—C13A 1.395 (2)
O1B—H1OB 0.84 (2) C12A—H12A 0.9300
N1B—C9B 1.4059 (17) C11B—C12B 1.374 (2)
N1B—C1B 1.4644 (18) C13A—C14A 1.360 (2)
N1B—H1NB 0.865 (17) C13A—H13A 0.9300
C1B—N2B 1.4638 (17) C12B—C13B 1.397 (3)
C1B—C2B 1.5013 (17) C12B—H12B 0.9300
C1B—H1B 0.9800 C14A—C15A 1.406 (2)
C3A—C4A 1.387 (2) C14A—H14A 0.9300
C2B—C7B 1.3833 (18) C13B—C14B 1.356 (3)
C2B—C3B 1.3949 (18) C13B—H13B 0.9300
N2B—C11B 1.3942 (17) C15A—C16A 1.412 (2)
N2B—H2NB 0.862 (17) C14B—C15B 1.421 (3)
C4A—C5A 1.381 (3) C14B—H14B 0.9300
C4A—H4A 0.9300 C16A—C17A 1.354 (2)
C3B—C4B 1.3840 (19) C16A—H16A 0.9300
C5A—C6A 1.368 (3) C15B—C16B 1.410 (3)
C5A—H5A 0.9300 C17A—C18A 1.401 (2)
C4B—C5B 1.373 (2) C17A—H17A 0.9300
C4B—H4B 0.9300 C16B—C17B 1.353 (3)
C6A—C7A 1.383 (2) C16B—H16B 0.9300
C6A—H6A 0.9300 C18A—H18A 0.9300
C5B—C6B 1.375 (2) C18B—C17B 1.406 (3)
C5B—H5B 0.9300 C18B—H18B 0.9300
C7A—H7A 0.9300 C17B—H17B 0.9300
N1A—C1A—N2A 106.61 (11) N1A—C9A—C10A 117.35 (11)
N1A—C1A—C2A 110.09 (11) C6B—C7B—C2B 121.03 (13)
N2A—C1A—C2A 109.23 (11) C6B—C7B—H7B 119.5
N1A—C1A—H1A 110.3 C2B—C7B—H7B 119.5
N2A—C1A—H1A 110.3 C11A—C10A—C9A 120.35 (11)
C2A—C1A—H1A 110.3 C11A—C10A—C15A 119.31 (12)
C9A—N1A—C1A 117.08 (11) C9A—C10A—C15A 120.30 (11)
C9A—N1A—H1N1 115.0 (12) C18B—C9B—N1B 122.14 (15)
C1A—N1A—H1N1 112.7 (12) C18B—C9B—C10B 120.75 (14)
C3A—O1A—H1OA 106.1 (14) N1B—C9B—C10B 117.02 (13)
C7A—C2A—C3A 118.36 (13) C12A—C11A—N2A 121.94 (12)
C7A—C2A—C1A 120.67 (13) C12A—C11A—C10A 120.34 (12)
C3A—C2A—C1A 120.97 (12) N2A—C11A—C10A 117.56 (12)
C11A—N2A—C1A 117.26 (10) C9B—C10B—C11B 120.84 (12)
C11A—N2A—H1NA 112.9 (12) C9B—C10B—C15B 119.55 (15)
C1A—N2A—H1NA 111.1 (12) C11B—C10B—C15B 119.53 (15)
C3B—O1B—H1OB 107.7 (17) C11A—C12A—C13A 119.88 (14)
C9B—N1B—C1B 114.90 (11) C11A—C12A—H12A 120.1
C9B—N1B—H1NB 113.0 (10) C13A—C12A—H12A 120.1
C1B—N1B—H1NB 112.5 (10) C12B—C11B—N2B 122.37 (15)
N2B—C1B—N1B 106.09 (10) C12B—C11B—C10B 120.51 (14)
N2B—C1B—C2B 110.09 (11) N2B—C11B—C10B 117.02 (12)
N1B—C1B—C2B 110.99 (10) C14A—C13A—C12A 121.31 (14)
N2B—C1B—H1B 109.9 C14A—C13A—H13A 119.3
N1B—C1B—H1B 109.9 C12A—C13A—H13A 119.3
C2B—C1B—H1B 109.9 C11B—C12B—C13B 119.89 (19)
O1A—C3A—C4A 117.37 (13) C11B—C12B—H12B 120.1
O1A—C3A—C2A 122.12 (12) C13B—C12B—H12B 120.1
C4A—C3A—C2A 120.50 (14) C13A—C14A—C15A 120.62 (13)
C7B—C2B—C3B 118.45 (12) C13A—C14A—H14A 119.7
C7B—C2B—C1B 120.52 (11) C15A—C14A—H14A 119.7
C3B—C2B—C1B 121.02 (11) C14B—C13B—C12B 121.03 (18)
C11B—N2B—C1B 116.45 (11) C14B—C13B—H13B 119.5
C11B—N2B—H2NB 114.1 (10) C12B—C13B—H13B 119.5
C1B—N2B—H2NB 114.4 (10) C14A—C15A—C16A 123.37 (13)
C5A—C4A—C3A 119.71 (16) C14A—C15A—C10A 118.52 (12)
C5A—C4A—H4A 120.1 C16A—C15A—C10A 118.08 (13)
C3A—C4A—H4A 120.1 C13B—C14B—C15B 121.50 (16)
O1B—C3B—C4B 117.87 (12) C13B—C14B—H14B 119.3
O1B—C3B—C2B 121.81 (12) C15B—C14B—H14B 119.3
C4B—C3B—C2B 120.30 (12) C17A—C16A—C15A 120.50 (13)
C6A—C5A—C4A 120.55 (14) C17A—C16A—H16A 119.8
C6A—C5A—H5A 119.7 C15A—C16A—H16A 119.8
C4A—C5A—H5A 119.7 C16B—C15B—C14B 124.57 (18)
C5B—C4B—C3B 120.04 (14) C16B—C15B—C10B 117.87 (18)
C5B—C4B—H4B 120.0 C14B—C15B—C10B 117.52 (18)
C3B—C4B—H4B 120.0 C16A—C17A—C18A 121.78 (13)
C5A—C6A—C7A 119.76 (16) C16A—C17A—H17A 119.1
C5A—C6A—H6A 120.1 C18A—C17A—H17A 119.1
C7A—C6A—H6A 120.1 C17B—C16B—C15B 121.10 (17)
C4B—C5B—C6B 120.27 (13) C17B—C16B—H16B 119.4
C4B—C5B—H5B 119.9 C15B—C16B—H16B 119.4
C6B—C5B—H5B 119.9 C9A—C18A—C17A 119.91 (14)
C6A—C7A—C2A 121.10 (15) C9A—C18A—H18A 120.0
C6A—C7A—H7A 119.4 C17A—C18A—H18A 120.0
C2A—C7A—H7A 119.4 C9B—C18B—C17B 118.95 (19)
C5B—C6B—C7B 119.85 (14) C9B—C18B—H18B 120.5
C5B—C6B—H6B 120.1 C17B—C18B—H18B 120.5
C7B—C6B—H6B 120.1 C16B—C17B—C18B 121.76 (19)
C18A—C9A—N1A 123.03 (13) C16B—C17B—H17B 119.1
C18A—C9A—C10A 119.42 (12) C18B—C17B—H17B 119.1
N2A—C1A—N1A—C9A 53.40 (15) C1A—N2A—C11A—C10A 27.40 (17)
C2A—C1A—N1A—C9A 171.78 (12) C9A—C10A—C11A—C12A −177.51 (12)
N1A—C1A—C2A—C7A 110.84 (15) C15A—C10A—C11A—C12A 0.02 (18)
N2A—C1A—C2A—C7A −132.41 (14) C9A—C10A—C11A—N2A −1.84 (18)
N1A—C1A—C2A—C3A −68.59 (16) C15A—C10A—C11A—N2A 175.69 (11)
N2A—C1A—C2A—C3A 48.16 (16) C18B—C9B—C10B—C11B 177.89 (14)
N1A—C1A—N2A—C11A −50.96 (15) N1B—C9B—C10B—C11B 1.32 (18)
C2A—C1A—N2A—C11A −169.89 (11) C18B—C9B—C10B—C15B 1.2 (2)
C9B—N1B—C1B—N2B 57.04 (13) N1B—C9B—C10B—C15B −175.39 (12)
C9B—N1B—C1B—C2B 176.61 (11) N2A—C11A—C12A—C13A −174.43 (13)
C7A—C2A—C3A—O1A −177.96 (13) C10A—C11A—C12A—C13A 1.0 (2)
C1A—C2A—C3A—O1A 1.5 (2) C1B—N2B—C11B—C12B −155.68 (12)
C7A—C2A—C3A—C4A 1.3 (2) C1B—N2B—C11B—C10B 27.86 (16)
C1A—C2A—C3A—C4A −179.23 (13) C9B—C10B—C11B—C12B −175.50 (12)
N2B—C1B—C2B—C7B −118.22 (14) C15B—C10B—C11B—C12B 1.21 (19)
N1B—C1B—C2B—C7B 124.63 (13) C9B—C10B—C11B—N2B 1.03 (18)
N2B—C1B—C2B—C3B 61.14 (16) C15B—C10B—C11B—N2B 177.74 (12)
N1B—C1B—C2B—C3B −56.01 (16) C11A—C12A—C13A—C14A −0.9 (2)
N1B—C1B—N2B—C11B −55.21 (14) N2B—C11B—C12B—C13B −177.43 (13)
C2B—C1B—N2B—C11B −175.37 (11) C10B—C11B—C12B—C13B −1.1 (2)
O1A—C3A—C4A—C5A 178.05 (14) C12A—C13A—C14A—C15A −0.3 (2)
C2A—C3A—C4A—C5A −1.3 (2) C11B—C12B—C13B—C14B −0.3 (3)
C7B—C2B—C3B—O1B −176.49 (14) C13A—C14A—C15A—C16A 179.26 (14)
C1B—C2B—C3B—O1B 4.1 (2) C13A—C14A—C15A—C10A 1.3 (2)
C7B—C2B—C3B—C4B 2.2 (2) C11A—C10A—C15A—C14A −1.20 (18)
C1B—C2B—C3B—C4B −177.14 (13) C9A—C10A—C15A—C14A 176.34 (12)
C3A—C4A—C5A—C6A 0.3 (3) C11A—C10A—C15A—C16A −179.24 (11)
O1B—C3B—C4B—C5B 176.17 (15) C9A—C10A—C15A—C16A −1.70 (18)
C2B—C3B—C4B—C5B −2.6 (2) C12B—C13B—C14B—C15B 1.5 (3)
C4A—C5A—C6A—C7A 0.5 (3) C14A—C15A—C16A—C17A −176.90 (14)
C3B—C4B—C5B—C6B 0.8 (2) C10A—C15A—C16A—C17A 1.0 (2)
C5A—C6A—C7A—C2A −0.4 (3) C13B—C14B—C15B—C16B 176.13 (19)
C3A—C2A—C7A—C6A −0.5 (2) C13B—C14B—C15B—C10B −1.3 (3)
C1A—C2A—C7A—C6A −179.92 (14) C9B—C10B—C15B—C16B −0.9 (2)
C4B—C5B—C6B—C7B 1.4 (3) C11B—C10B—C15B—C16B −177.64 (15)
C1A—N1A—C9A—C18A 153.25 (13) C9B—C10B—C15B—C14B 176.72 (14)
C1A—N1A—C9A—C10A −31.88 (17) C11B—C10B—C15B—C14B 0.0 (2)
C5B—C6B—C7B—C2B −1.7 (2) C15A—C16A—C17A—C18A −0.2 (2)
C3B—C2B—C7B—C6B −0.1 (2) C14B—C15B—C16B—C17B −176.93 (19)
C1B—C2B—C7B—C6B 179.29 (14) C10B—C15B—C16B—C17B 0.5 (3)
C18A—C9A—C10A—C11A 179.05 (12) N1A—C9A—C18A—C17A 174.10 (13)
N1A—C9A—C10A—C11A 3.99 (17) C10A—C9A—C18A—C17A −0.7 (2)
C18A—C9A—C10A—C15A 1.53 (19) C16A—C17A—C18A—C9A 0.0 (2)
N1A—C9A—C10A—C15A −173.53 (11) N1B—C9B—C18B—C17B 175.37 (15)
C1B—N1B—C9B—C18B 151.26 (14) C10B—C9B—C18B—C17B −1.0 (2)
C1B—N1B—C9B—C10B −32.21 (16) C15B—C16B—C17B—C18B −0.4 (3)
C1A—N2A—C11A—C12A −157.00 (13) C9B—C18B—C17B—C16B 0.6 (3)