Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [Cu(C15HF10O2)2]·3(C6H6O2S) |
| M r | 1296.36 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 7.7343 (3), 46.8973 (16), 13.2580 (5) |
| β (°) | 99.211 (1) |
| V (Å3) | 4746.9 (3) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.73 |
| Crystal size (mm) | 0.17 × 0.17 × 0.11 |
| Data collection | |
| Diffractometer | Bruker D8 Goniometer |
| Absorption correction | Multi-scan (SADABS; Bruker, 2018 ▸) |
| T min, T max | 0.88, 0.93 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 54634, 8367, 7663 |
| R int | 0.042 |
| (sin θ/λ)max (Å−1) | 0.595 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.049, 0.106, 1.06 |
| No. of reflections | 8367 |
| No. of parameters | 821 |
| No. of restraints | 236 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 1.74, −1.69 |