| Crystal data |
| Chemical formula |
C22H25NOS |
|
M
r
|
351.49 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
150 |
|
a, b, c (Å) |
8.8581 (19), 9.183 (2), 13.021 (3) |
| α, β, γ (°) |
106.474 (3), 109.398 (3), 93.383 (3) |
|
V (Å3) |
944.2 (4) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.18 |
| Crystal size (mm) |
0.33 × 0.26 × 0.10 |
| |
| Data collection |
| Diffractometer |
Bruker Smart APEX CCD |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.83, 0.98 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
17663, 4860, 3807 |
|
R
int
|
0.029 |
| (sin θ/λ)max (Å−1) |
0.677 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.046, 0.134, 1.08 |
| No. of reflections |
4860 |
| No. of parameters |
228 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.54, −0.22 |
