Table 1. Hydrogen-bond geometry (Å, °).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| N11—H11⋯O42i | 0.84 (2) | 2.20 (2) | 3.025 (2) | 169.6 (18) |
| O41—H41⋯N22ii | 1.01 | 1.78 | 2.6566 (19) | 144 |
| O30—H30⋯N1 | 0.99 (3) | 1.65 (3) | 2.6135 (19) | 166 (2) |
| C5—H5⋯O42i | 0.95 | 2.25 | 3.194 (2) | 170 |
| C2—H2⋯F1iii | 0.95 | 2.15 | 3.07 (3) | 163 |
| C2—H2⋯F1′iii | 0.95 | 2.32 | 3.253 (3) | 166 |
| C29—H29B⋯O18iv | 0.98 | 2.65 | 3.6101 (19) | 167 |
| C23—H23B⋯O25v | 0.99 | 2.57 | 3.220 (2) | 123 |
| C27—H27B⋯F1vi | 0.99 | 2.71 | 3.68 (4) | 166 |
| C39—H39A⋯O30vii | 0.99 | 2.50 | 3.255 (4) | 133 |
| C21—H21B⋯O31viii | 0.99 | 2.29 | 3.234 (2) | 160 |
| C13—H13⋯O30ix | 0.95 | 2.39 | 3.139 (3) | 135 |
| C13′—H13′⋯O30ix | 0.95 | 2.53 | 3.268 (3) | 135 |
| Cg2⋯Cg2viii | 3.5358 (11) | 0 (1) | ||
| Cg2⋯Cg3viii | 3.7909 (11) | 1 (1) | ||
| Cg2⋯Cg3ix | 3.7530 (11) | 1 (1) | ||
| Cg3⋯Cg3viii | 3.7934 (11) | 0 (1) |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
; (vii)
; (viii)
; (ix)
.