| Refinement on F2 | Hydrogen site location: inferred from neighbouring sites |
| Least-squares matrix: full | H-atom parameters constrained |
| R[F2 > 2σ(F2)] = 0.021 | w = 1/[σ2(Fo2) + (0.0232P)2 + 0.1399P] where P = (Fo2 + 2Fc2)/3 |
| wR(F2) = 0.054 | (Δ/σ)max = 0.002 |
| S = 1.08 | Δρmax = 0.68 e Å−3 |
| 4238 reflections | Δρmin = −0.52 e Å−3 |
| 111 parameters | Extinction correction: SHELXL-2017/1 (Sheldrick 2015b), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
| 0 restraints | Extinction coefficient: 0.018 (2) |