| Crystal data |
| Chemical formula |
[Cu2Cl4(C7H8N2)2] |
|
M
r
|
509.19 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
7.7054 (5), 7.7240 (5), 8.5606 (5) |
| α, β, γ (°) |
103.659 (5), 98.803 (5), 110.273 (5) |
|
V (Å3) |
448.74 (5) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
2.97 |
| Crystal size (mm) |
0.56 × 0.41 × 0.16 |
| |
| Data collection |
| Diffractometer |
Oxford Diffraction Gemini diffractometer |
| Absorption correction |
Analytical (CrysAlis PRO; Rigaku OD, 2016 ▸) |
|
T
min, T
max
|
0.367, 0.669 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
13153, 4238, 3866 |
|
R
int
|
0.024 |
| (sin θ/λ)max (Å−1) |
0.827 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.021, 0.054, 1.08 |
| No. of reflections |
4238 |
| No. of parameters |
111 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.68, −0.52 |
