Table 1.
Position | δ C a,b | δH a,c (mult, J in Hz) | HMBC |
---|---|---|---|
2 | 77.3 | 4.72 (m) | |
3 | 43.5 | 2.53 (m) | 2, 4, 11 |
4 | 191.0 | - | - |
4a | 102.4 | - | - |
5 | 64.1 | 5.03 (d, 12.0),4.73 (d, 12.0) | 4, 4a, 6a, 10b |
6a | 156.3 | - | - |
7 | 104.8 | 6.34 (s) | 6a, 8, 9, 10, 10b |
8 | 154.5 | - | - |
9 | 144.8 | - | - |
10 | 108.9 | 7.06 (s) | 6a, 8, 9, 10, 10b |
10a | 107.9 | - | |
10b | 165.7 | - | - |
11 | 20.6 | 1.55 (d, 6.4) | 2, 3, 4 |
12 | 57.0 | 3.83 (s) | 9 |
a Recorded in CD3OD, b 100 MHz, c 400 MHz.