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. 2020 May 21;25(10):2405. doi: 10.3390/molecules25102405

Table 2.

13C-NMR data (75 MHz, CDCl3) for 36, 8, 1015.

Position δC (ppm)
3 4 5 6 8
C-1 131.2 130.7 137.0 136.8 139.6
C-2 115.2 114.9 117.8 116.5 111.9
C-3 150.4 149.8 154.3 153.8 156.3
C-4 130.7 130.7 139.8 139.7 137.6
C-4a 147.5 147.4 151.6 151.4 150.5
C-5 117.5 101.6 117.6 99.7 99.8
C-6 134.4 162.9 134.6 164.8 165.4
C-7 123.7 113.3 124.4 113.6 114.0
C-8 126.0 127.9 127.1 128.5 128.6
C-8a 121.8 114.9 122.7 117.7 116.1
C-9 176.9 176.2 177.8 176.9 177.1
C-9a 112.8 112.6 117.8 118.0 111.0
C-10a 154.7 156.5 154.9 156.6 157.0
C-1′ - - - - 39.5
1-CH3 22.4 22.4 21.7 21.5 -
3-OCH3 - - 62.0 61.9 56.7
4-OCH3 - - 61.4 61.2 61.8
6-OCH3 - - - 55.9 56.1
Position 10 12 13 14 15
C-1 133.6 128.7 129.8 129.7 129.7
C-2 108.3 115.5 108.4 107.7 106.8
C-3 156.0 156.3 156.3 156.5 156.1
C-4 140.7 140.0 138.0 137.5 136.9
C-4a 150.9 152.1 150.5 150.5 150.7
C-5 100.1 99.3 118.5 100.4 121.4
C-6 165.5 157.4 135.5 165.3 135.3
C-7 114.2 117.9 121.9 113.9 124.4
C-8 128.3 129.2 130.8 128.3 126.1
C-8a 115.9 113.8 124.9 115.3 117.8
C-9 177.1 178.8 176.0 174.7 177.0
C-9a 116.4 114.1 114.3 113.9 113.2
C-10a 157.5 165.6 157.3 157.8 154.7
C-1′ 193.1 166.9 170.4 170.1 147.9
1-CH3 - - - - -
3-OCH3 56.7 61.9 62.3 61.8 56.3
4-OCH3 61.9 56.9 57.2 56.7 61.1
6-OCH3 56.1 56.4 - 56.1 -