Table 2.
Position | δC (ppm) | ||||
---|---|---|---|---|---|
3 | 4 | 5 | 6 | 8 | |
C-1 | 131.2 | 130.7 | 137.0 | 136.8 | 139.6 |
C-2 | 115.2 | 114.9 | 117.8 | 116.5 | 111.9 |
C-3 | 150.4 | 149.8 | 154.3 | 153.8 | 156.3 |
C-4 | 130.7 | 130.7 | 139.8 | 139.7 | 137.6 |
C-4a | 147.5 | 147.4 | 151.6 | 151.4 | 150.5 |
C-5 | 117.5 | 101.6 | 117.6 | 99.7 | 99.8 |
C-6 | 134.4 | 162.9 | 134.6 | 164.8 | 165.4 |
C-7 | 123.7 | 113.3 | 124.4 | 113.6 | 114.0 |
C-8 | 126.0 | 127.9 | 127.1 | 128.5 | 128.6 |
C-8a | 121.8 | 114.9 | 122.7 | 117.7 | 116.1 |
C-9 | 176.9 | 176.2 | 177.8 | 176.9 | 177.1 |
C-9a | 112.8 | 112.6 | 117.8 | 118.0 | 111.0 |
C-10a | 154.7 | 156.5 | 154.9 | 156.6 | 157.0 |
C-1′ | - | - | - | - | 39.5 |
1-CH3 | 22.4 | 22.4 | 21.7 | 21.5 | - |
3-OCH3 | - | - | 62.0 | 61.9 | 56.7 |
4-OCH3 | - | - | 61.4 | 61.2 | 61.8 |
6-OCH3 | - | - | - | 55.9 | 56.1 |
Position | 10 | 12 | 13 | 14 | 15 |
C-1 | 133.6 | 128.7 | 129.8 | 129.7 | 129.7 |
C-2 | 108.3 | 115.5 | 108.4 | 107.7 | 106.8 |
C-3 | 156.0 | 156.3 | 156.3 | 156.5 | 156.1 |
C-4 | 140.7 | 140.0 | 138.0 | 137.5 | 136.9 |
C-4a | 150.9 | 152.1 | 150.5 | 150.5 | 150.7 |
C-5 | 100.1 | 99.3 | 118.5 | 100.4 | 121.4 |
C-6 | 165.5 | 157.4 | 135.5 | 165.3 | 135.3 |
C-7 | 114.2 | 117.9 | 121.9 | 113.9 | 124.4 |
C-8 | 128.3 | 129.2 | 130.8 | 128.3 | 126.1 |
C-8a | 115.9 | 113.8 | 124.9 | 115.3 | 117.8 |
C-9 | 177.1 | 178.8 | 176.0 | 174.7 | 177.0 |
C-9a | 116.4 | 114.1 | 114.3 | 113.9 | 113.2 |
C-10a | 157.5 | 165.6 | 157.3 | 157.8 | 154.7 |
C-1′ | 193.1 | 166.9 | 170.4 | 170.1 | 147.9 |
1-CH3 | - | - | - | - | - |
3-OCH3 | 56.7 | 61.9 | 62.3 | 61.8 | 56.3 |
4-OCH3 | 61.9 | 56.9 | 57.2 | 56.7 | 61.1 |
6-OCH3 | 56.1 | 56.4 | - | 56.1 | - |