Table 3.
DTA instrument parameters.
Data Collection properties | Settings | |
---|---|---|
Sample | Sample type | Powder |
Sample pre-treatment | Grinding | |
Sample holder material | Alumina | |
Minimum sample weight | 50 mg | |
Test parameters | Temperature range | 40°C to 10000C |
Heat rate | 200C/min | |
Purging gas | N2 (Nitrogen) | |
Gas flow rate | 30 mL/min | |
Total measurement | 90 min |