Maceration |
≤boiling point |
atmospheric |
e.g., flask |
any solvent |
sample is extracted by soaking in solvent |
Refluxing |
≤boiling point |
atmospheric |
round bottomed flask |
any solvent |
maceration on increased temperature, vaporization of solvent is avoided by condensation |
Soxhlet |
≤boiling point |
atmospheric |
Soxhlet cartridge |
any solvent |
special form of percolation (continuous) |
Percolation |
room temperature |
atmospheric |
e.g., column |
any solvent |
sample placed in column, solvent is added, flow through and is released |
Sonication |
room temperature |
atmospheric |
e.g., flask |
any solvent |
maceration assisted by sonication to increase solubility |
SFE (Supercritical Fluid Extraction) |
>boiling point |
pressurized |
reaction vessel |
e.g., CO2
|
temperature and pressure above critical point to control extraction characteristics |
PLE (Pressurized Liquid Extraction) |
>boiling point |
pressurized |
reaction vessel |
no corrosive/decomposing solvents |
pressurization allows temperatures above boiling point, faster extractions |
MAE (Microwave Assisted Extraction) |
>boiling point |
atmospheric |
reaction vessel |
no decomposing solvents |
pressurization or pressure stabile reaction vessels allow temperatures above boiling point, faster extractions heated by radiation |
HPPE (High Pressure Propane Extraction) |
>boiling point |
pressurized |
reaction vessel |
propane |
variation of SFE |
Cold Ion Exchange |
room temperature |
atmospheric |
column |
any solvent |
plant material placed in column solvent is pumped continues in cycle, analyte is adsorbed on specific material |
PHWE (Pressurized Hot Water Extraction) |
>boiling point |
pressurized |
column |
water (different modifier) |
sample is placed in column, hot water (modifier) is pumped through column |