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. 2020 May 13;12(5):320. doi: 10.3390/toxins12050320

Table 1.

Concise description of extraction techniques used. All technical variations are based on maceration or percolation.

Technique Temperature Pressure Sample Solvent Remarks
Maceration ≤boiling point atmospheric e.g., flask any solvent sample is extracted by soaking in solvent
Refluxing ≤boiling point atmospheric round bottomed flask any solvent maceration on increased temperature, vaporization of solvent is avoided by condensation
Soxhlet ≤boiling point atmospheric Soxhlet cartridge any solvent special form of percolation (continuous)
Percolation room temperature atmospheric e.g., column any solvent sample placed in column, solvent is added, flow through and is released
Sonication room temperature atmospheric e.g., flask any solvent maceration assisted by sonication to increase solubility
SFE (Supercritical Fluid Extraction) >boiling point pressurized reaction vessel e.g., CO2 temperature and pressure above critical point to control extraction characteristics
PLE (Pressurized Liquid Extraction) >boiling point pressurized reaction vessel no corrosive/decomposing solvents pressurization allows temperatures above boiling point, faster extractions
MAE (Microwave Assisted Extraction) >boiling point atmospheric reaction vessel no decomposing solvents pressurization or pressure stabile reaction vessels allow temperatures above boiling point, faster extractions heated by radiation
HPPE (High Pressure Propane Extraction) >boiling point pressurized reaction vessel propane variation of SFE
Cold Ion Exchange room temperature atmospheric column any solvent plant material placed in column solvent is pumped continues in cycle, analyte is adsorbed on specific material
PHWE (Pressurized Hot Water Extraction) >boiling point pressurized column water (different modifier) sample is placed in column, hot water (modifier) is pumped through column