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. 2020 May 13;12(5):320. doi: 10.3390/toxins12050320

Table 7.

Overview on the extraction experiments for Senecio by Hartmann et al. Results correspond to the content of free PA bases determined by GC-MS, and N-oxides by HPLC-UV [72]. Missing information is characterized by “--”.

Technique Sample
(g)
Volume (mL) Time (h) Temperature (°C) Solvent Result (%)
1 Maceration 6–10 20 0.5 Room Temperature Sulfuric Acid 0.1 N 5 *
2 Soxhlet -- -- 48 Boiling Point Methanol 44 *

* percentage of free bases with reference to the overall PA content.