Table 15.
Overview on the extraction experiments by Jiang et al. to investigate the influence of different extraction techniques on the yield of senecionine and senkirkine extracted from Tussilago. The result correspond to the sum of senecionine and senkirkine determined by LC/MS/MS [157].
| Technique | Sample (g) |
Volume (mL) |
Time (min) |
Temperature (°C) |
Solvent | Result (ppm) | |
|---|---|---|---|---|---|---|---|
| 1 | MAE | 1 | 40 | 15 | Bp. | Water/Methanol acidified with HCl | 104.4 |
| 2 | Reflux | 1 | 60 | 60 | Bp. | 1 N HCl | 109.6 |
| 3 | PHWE | 0.25 | 50 | 50 | 60 | Water | 88.2 |
| 4 | Reflux | 1 | 60 | 60 | Bp. | 1 N HCl | 87.9 |