Table 1. 13C (100 and 125 MHz) NMR Spectroscopic Data for Compounds 1–6 in CDCl3.
no | 1 | 2a | 3 | 4 | 5 | 6 |
---|---|---|---|---|---|---|
1 | 40.2 | 45.3 | 47.1 | 55.4 | 39.4 | 33.6 |
2 | 134.3 | 173.0b | 213.5 | 213.2 | 152.8 | 52.7 |
3 | 133.2 | 101.8b | 47.0 | 49.4 | 147.8 | 74.1 |
4 | 28.9 | 22.2 | 30.6 | 32.2 | 18.1 | 33.0 |
5 | 22.8 | 33.6 | 37.5 | 26.4 | 26.3 | 32.9 |
6 | 82.3 | 67.5 | 75.5 | 84.6 | 83.5 | 215.9 |
7 | 37.7 | 31.7 | 84.0 | 69.4 | 69.9 | 50.5 |
8 | 31.7 | 32.2 | 27.7 | 32.8 | 34.3 | 29.9 |
9 | 27.3 | 26.1 | 29.8 | 20.9 | 20.6 | 23.7 |
10 | 83.2 | 92.3 | 85.6 | 73.4 | 72.7 | 82.6 |
11 | 39.3 | 40.0 | 39.6 | 39.9 | 36.1 | 39.5 |
12 | 168.8 | 170.6b | 19.3 | 20.7 | 195.7 | 68.3 |
13 | 20.4 | 14.2 | 20.9 | 24.7 | 23.7 | 30.6 |
14 | 25.9 | 29.2 | 27.7 | 27.3 | 23.7 | 33.2 |
15 | 22.0 | 21.9 | 27.6 | 21.1 | 22.2 | 29.2 |
13C NMR (125 MHz).
13C NMR (200 MHz).