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. 2020 Apr 14;22(9):3697–3701. doi: 10.1021/acs.orglett.0c01182

Scheme 3. Application of Various Aldehydes.

Scheme 3

Conditions: olefin (0.5 mmol, 1 equiv), TBPB (2 equiv), Ir(ppy)3 (0.4 mol %), aldehyde (5 equiv), N-methylindole (3 equiv), NaHCO3 (2 equiv), MeCN (5 mL), white LED light, 65 °C, 12 h.