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. Author manuscript; available in PMC: 2020 Jun 21.
Published in final edited form as: Biochemistry. 2020 Apr 30;59(19):1800–1803. doi: 10.1021/acs.biochem.0c00091

Figure 3.

Figure 3.

Overlaid two-dimensional 13C-13C correlation solid-state NMR spectra for the native (red) and amyloid (black) states of TTRwt formed at pH 4.4 obtained at a proton frequency of 800 MHz. A dipolar-assist rotational resonance (DARR) with 20 ms mixing time was used for the mixing scheme.