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. 2020 Mar 5;59(6):3993–4001. doi: 10.1021/acs.inorgchem.9b03664

Figure 3.

Figure 3

1H NMR spectra (500 MHz, acetone-d6, 296 K): (a) free ligand 2; (b) pure [Ag4F(2)2](OTf)3; (c) mixture of [Ag5F(2)2](OTf)4 and [Ag4F(2)2](OTf)3 resulting from 2/1/1 [AgOTf]/[2]/[AgF]; (d) pure [Ag5F(2)2](OTf)4.