Table 2. Single-crystal data sets collected for the five samples of this study, using five different setups [(1)–(5)].
The number of diffraction patterns per data set, the resolution range (d spacing), the average number of experimental peaks per frame and the number of independent reflections expected in the resolution range are indicated.
| Data set name | Monochromatic | 4% | 50% | LaueDET-50/60 | LaueDET-90 | |
|---|---|---|---|---|---|---|
| Energy range (keV) | 17.75 | 16.9–17.7 | 10–17 | 5–24 | 5–24 | |
| Setup No. | (1) | (2) | (3) | (4) | (5) | |
| Sanidine | No. patterns | 100 | 85 | 80 | 10 | |
| Resolution range (Å−1) | Inf–0.450 | 3.599–0.406 | 5.872–0.312 | 1.563–0.227 | ||
| Average No. peaks per frame | 16 | 67 | 98 | 201 | ||
| No. independent reflections | 4337 | 5809 | 12 674 | 32 313 | ||
| CsPt | No. patterns | 100 | 100 | 12 | ||
| Resolution range (Å−1) | Inf–0.574 | Inf–0.560 | 5.950–0.315 | |||
| Average No. peaks per frame | 9 | 16 | 353 | |||
| No. independent reflections | 523 | 551 | 2715 | |||
| ZrPOF | No. patterns | 21 | 17 | |||
| Resolution range (Å−1) | Inf–0.510 | 5.878–0.313 | ||||
| Average No. peaks per frame | 34 | 170 | ||||
| No. independent reflections | 7767 | 33 884 | ||||
| ZSM-5 | No. patterns | 100 | 100 | 17 | 15 | 19 |
| Resolution range (Å−1) | Inf–0.552 | Inf–0.559 | 3.471–0.387 | 4.155–0.287 | 1.685–0.230 | |
| Average No. peaks per frame | 12 | 26 | 148 | 472 | 517 | |
| No. independent reflections | 4604 | 4427 | 12 884 | 31 063 | 59 358 | |
| MgAc | No. patterns | 29 | 37 | |||
| Resolution range (Å−1) | 3.599–0.406 | 1.670–0.229 | ||||
| Average No. peaks per frame | 118 | 213 | ||||
| No. independent reflections | 7150 | 37 989 | ||||