Table 4. Fine slicing experiment for FeSb2 .
Beam flux (%)† | Temperature (K) | Exposure time (s) | Speed (s per °) | Slicing (°) | Strategy |
---|---|---|---|---|---|
12 | 100 | 0.10 | 2.0 | 0.05 | ‡ |
12 | 100 | 0.20 | 2.0 | 0.10 | ‡ |
12 | 100 | 1.00 | 2.0 | 0.50 | ‡ |
100 | 100 | 0.01 | 1.0 | 0.01 | ‡ § |
100 | 100 | 0.10 | 2.0 | 0.05 | ‡ |
100 | 100 | 0.20 | 2.0 | 0.10 | ‡ |
100 | 100 | 1.00 | 2.0 | 0.50 | ‡ |
As a percentage of the maximum beam flux.
180° ω scan at χ = 0.0, 20.0 and 45.0° and 2θ = 0.0, −20.0° (six runs).
Due to an experimental error, the data were only collected up to 36° in ω per run.