Table 7. Comparison of the quality of FeSb2 models† with and without a refined extinction parameter.
| Beam flux (%)‡ | GoF | Data | Extinction (%)§ | R(F 2) (%) | egross |
|---|---|---|---|---|---|
| 12 | 0.9657 | 2497 | 8.1 | 1.51 | 16.66 |
| 12 | 0.9896 | 2497 | None | 1.76 | 18.56 |
| 31 | 0.9592 | 2493 | 10.3 | 1.53 | 16.05 |
| 31 | 0.994 | 2493 | None | 1.87 | 19.95 |
| 65 | 1.0003 | 2504 | 20.6 | 1.45 | 15.00 |
| 65 | 1.1684 | 2504 | None | 2.43 | 27.14 |
| 100 | 1.0304 | 2506 | 30.7 | 1.32 | 14.10 |
| 100 | 1.5559 | 2506 | None | 3.15 | 36.83 |
†
Collected with 1.0 s exposure time, using the recurrence background method and without profile fitting.
‡
As a percentage of the maximum beam flux.
§
Given as the maximum percentage reduction of an individual reflection intensity (always the 120 reflection).