Table 1. Optimization of the Reaction Conditionsa.
Reactions performed at 0.025 mmol of 1a. Yields determined by 19F NMR using 1-fluoro-4-nitrobenzene as internal standard.
Isolated yield of pure material of a reaction performed at 0.3 mmol of 1a.
Reactions performed at 0.025 mmol of 1a. Yields determined by 19F NMR using 1-fluoro-4-nitrobenzene as internal standard.
Isolated yield of pure material of a reaction performed at 0.3 mmol of 1a.