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13C–1H HETCOR (contact time 100 μs) NMR spectrum for CO2-dosed e-2-OH–Mg2(dobpdc). A single dominant correlation is observed at a 1H shift of 11.4 ppm and a 13C shift of 158.6 ppm, assigned to a carbamic acid –COOH group. Small correlations are observed at lower 1H chemical shifts regions that likely correspond to alcoholamine protons.
