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. 2020 Apr 14;59(26):10519–10522. doi: 10.1002/anie.202002366

Table 3.

NMR data, recorded in a mixture of HF and SO2 at −40°C; chemical shifts δ in ppm.

 

13C

14N

 

K4Mo(CN)8 in D2O

+149

−95

 

K4W(CN)8 in D2O

+143

−98

 

[Mo(CNH)8]4+ [SbF6]− 4 in HF

+121

−182

 

[W(CNH)8]4+ [SbF6]−4 in HF

+115

−179