Table 1.
I: | REDOR and 13C CP/MAS NMR Experiments | Distance * |
---|---|---|
1 | (E)4(A)6GGAGQGGYGGLGSQGAGRGGLGGQGAG(A)6(E)4 | |
2 | (E)4(A)6GGA[1-13C]G14Q[15N]G15GYGGLGSQGAGRGGLGGQGAG(A)6(E)4 | 3.71 Å |
3 | (E)4(A)6GGAGQG[1-13C]G17Y[15N]G19GLGSQGAGRGGLGGQGAG(A)6(E)4 | 3.97 Å |
4 | (E)4(A)6GGAGQGGYG[1-13C]G20L[15N]G22SQGAGRGGLGGQGAG(A)6(E)4 | 3.41 Å |
5 | (E)4(A)6GGAGQGGYGGLGSQGA[1-13C]G27R[15N]G29GLGGQGAG(A)6(E)4 | 3.64 Å |
6 | (E)4(A)6GGAGQGGYGGLGSQGAGRG[1-13C]G30L[15N]G32GQGAG(A)6(E)4 | 3.43 Å |
7 | (E)4(A)6GGAGQGGYGGLGSQGAGRGGLG[1-13C]G33Q[15N]35GAG(A)6(E)4 | 3.81 Å |
II: | 13 C CP/MAS NMR Experiment | |
8 | (E)4(A)6G [2-13C]G12 [3-13C]A13 [1-13C]G14QGGYGGLGSQGAGRGGLGGQGAG(A)6(E)4 | |
9 | (E)4(A)6GGAGQGGYGGLGSQ [2-13C]G25 [3-13C]A26 [1-13C]G27RGGLGGQGAG(A)6(E)4 | |
10 | (E)4(A)6GGAGQGGYGGLGSQGAGRGGLGGQ [2-13C]G35 [3-13C]A36 [1-13C]G37(A)6(E)4 |
Distance * is the inter-nuclear distance between 15N and 13C labeled sites [46].