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. 2020 Apr 21;64(6):569–585. doi: 10.1093/annweh/wxaa038

Table 3.

Summary of TDI exposure studies for the main processes.

Sector Study populations (country, no. workers) Biomonitoring data [expressed as range (median)] Notable correlations/comments LaKind scoringa References
Continuous foam production Poland (n = 20) Sum-TDA (U) = <0.01–3.9 µmol mol−1 cr. Positive for geometric mean (GM) in each group (r 0.9) U_totTDA (µmol mol−1) = 0.10777_TDI (µg m−3) + 0.2178 [5 ppb TDI = 4.1 µmol mol−1 cr.] RPE used and observed to impact TDA(U) results (no correlation between individual urinary TDA concentrations and TDI air concentrations). 12 Swierczynska-Machura et al. (2015)
UK (n = 26, 13 handlers, 13 non) Sum-TDA (U) = <~0.4 to 7 (2.21) µmol mol−1 cr. (handlers) No correlation between post-shift urinary TDA concentration and airborne TDI concentrations (r = 0.027). Dermal considered a significant factor—urine 20× higher for same airborne exposure. 16 Methodology not well described Austin (2007)
Belgiumb (n = 9) Sum-TDA (U) = 4.4–142.6 (18.01b) µg l−1 [21 samples] [~3 to ~97 (~12.3) µmol mol−1 cr.] TDA (µg g−1) = 0.547_TDI (µg m−3)–1.636, r = 0.917 [5 ppb TDI =19.2 µg g−1, 17.8 µmol mol−1 cr.] Proposed measuring ‘increase over shift’ to exclude accumulation. 12 External QA Geens et al. (2012)
Finland (n = 17) Sum-TDA (U) = <0.05 to 39 µmol mol−1 cr. Good correlation between airborne TDI and urinary TDA in post-shift samples (r = 0.91 and 0.86 for the two different factories studied). 13 Kääriä et al. (2001)
Sweden (n = 6) 2,4-TDA(U)/2,6-TDA(U) 0.5–5.4/0.2–4.7 µg l−1 [~0.3–3.7/0.14–3.2 µmol mol−1 cr.] 2,4-TDA(P)/2,6-TDA(P) 0.1–14/0.7–12 µg l−1 Samples taken Monday morning so results not comparable to other studies. Only reported levels ‘above reference value’. 12 Creatinine and specific gravity Tinnerberg et al. (2014)
Swedenc (n = 4 in 2000, n = 6 in 2005) 2,4-TDA (U) ~ 0–10 µmol mol−1 cr. 2,6-TDA (U) ~ 0–35 µmol mol−1 cr. 2,4-TDA (P)/2,6_pTDA (µg l−1) In 2000: 2.9–27.2 (7.0)/8.2–62.1 (30.8) In 2005: 0.5–1.3 (1.0)/2–11.8 (4.0) Urine results only presented graphically. 14 Small study Tinnerberg and Mattsson (2008)
Finland (n = 17) Sum-TDA(U) 0.2–39(4.9) µmol mol−1 cr. Sum-TDA(P) 0.4–70.8 (5.6) µg l−1 Sum_TDA(Hb) 0.012–0.33 (0.047) (nmol g−1) Air TDI and plasma TDA correlated (r = 0.91). Plasma and urine TDA well correlated (r = 0.97). 13 Säkkinen et al. (2011)
UK (n = 71) Sum-TDA(U) <0.5–15.5 (1.3) µmol mol−1 cr. 2,6-TDA(U) <0.5–13.2 (0.8) µmol mol−1 cr. 2,4-TDA (U) <0.5–5.6 (0.7) µmol mol−1 cr. The companies visited were involved in the manufacture of PUR products. 11 Cocker et al. (2009)
UK (n = 90) Sum-TDA(U) (µmol mol−1 cr.) <0.4–6.5 (90%, median <LOD) Positive association observed in 4 pairs of samples (air and urine). Air levels <LoD at 2/5 sites and only 1/11 samples >WEL (20 µg m−3 NCO)— no further data. 446 samples analysed of which 280 were below the detection limit. Follow-up to Cocker et al. (2009). 12 Keen et al. (2012)
Mixed Sweden (n = 136) (including: moulding-, continuous foam-, and flame-lamination plants) 2,6-TDA(U) <0.05–43.1 µg l−1 [~<0.03–29.3 µmol mol−1 cr.] 2,6-TDA(P) <0.05–62.1 µg l−1 Correlation (r > 0.86) with air levels for both urine and plasma for same-day samples. Same sites as Sennbro et al. (2004). 12 Littorin et al. (2007)
Sweden (n = 81) 2,4-TDA(U)/2,6-TDA(U)/Sum-TDA(U) <0.1–47 (4.5)/<0.1–115 (3.7)/<0.1–162 (9.7) µg l−1 [~<0.07–32 (3.1)/ −78 (2.5)/−110 (6.6) µmol mol−1 cr.] 2,4-TDA(P)/2,6-TDA(P)/Sum-TDA(P) <0.1–31 (7.4)/<0.1–42 (6.1)/<0.1–70 (14) µg l−1 High correlations between air exposure and urinary biomarker levels (ranging from 0.75 to 0.88) or plasma biomarker levels (ranging from 0.50 to 0.78). 2,6-TDA(U) (µg l−1) = 2.7_TDI(ppb) + 0.02 (r = 0.88) [5 ppb = 97 µg l−1, ~66 µmol mol−1 cr.] 13 Sennbro et al. (2004)
Japanb (n = 18) (spraying urethane paints) Individual results not reported except graphically, 2,6-TDA(U) <19 µmol mol−1 cr. 2,6-TDA(U) (µg g−1) = 6.6_TDI (ppb) –1.43 (r = 0.91) [5 ppb = 29 µmol mol−1 cr.] 13 Both raw and corrected data Sakai et al. (2005)
Finlandb (n = 6, car repair; n = 15 other PUR processes) Car repair Sum-TDA(U) <0.02–0.76 (0.23) µmol mol−1 cr. Other processes <0.02–0.17 (0.07) µmol mol−1 cr. Other processes included milling and turning of PUR-coated metal cylinders, injection moulding of thermoplastic PUR, welding of district heating pipes and joint welding of PUR floor covering. 11 Rosenberg et al. (2002)

aThe lower the LaKind score the better the overall quality (possible range 8–24).

bGeometric mean rather than median.

cCountry of origin assumed from authors’ affiliation, not specifically stated in paper.