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. 2020 Jun 18;31:105878. doi: 10.1016/j.dib.2020.105878

Table 1.

Results of validation process: LOQ, linearity, bias and precision (intraday and interday).

0.1 ng/ml
 0.5 ng/ml
 1 ng/ml
 5 ng/ml
 20 ng/ml
Precision (RSD. %)
 Precision (RSD. %)
 Precision (RSD. %)
 Precision (RSD. %)
 Precision (RSD. %)
N° Compound LOQ Linearity Bias (%) Intraday Interday Rec. (%) Intraday Interday Rec. (%) Intraday Interday Rec. (%) Intraday Interday Rec. (%) Intraday Interday
1 2-Phenylphenol 0.20 0.9946 N/A N/A N/A 110.10 8,99 11.18 100.03 8,25 6.86 86.09 6,67 8.32 100.98 13,03 1.62
2 4.4′-Dichlorobenzophenone (metabolite of dicofol) 0.80 0.9905 N/A N/A N/A N/A N/A N/A 100.35 8,41 12.21 101.69 6,90 17.71 96.39 13,85 1.72
3 Abamectine 4.00 0.9784 N/A N/A N/A N/A N/A N/A N/A N/A N/A 107.86 6,77 14.19 102.58 15,24 4.37
4 Acenaphthene 0.20 0.9889 N/A N/A N/A 83.21 17,09 8.12 124.25 9,64 7.02 94.92 6,78 10.11 96.71 7,51 8.70
5 Acenaphtylene 0.20 0.9792 N/A N/A N/A 108.10 14,25 15.63 99.81 10,39 5.64 94.84 15,98 10.11 102.65 7,26 9.23
6 Acephate 2.00 0.9879 N/A N/A N/A N/A N/A N/A N/A N/A N/A 119.99 13,67 0.16 103.25 7,44 12.14
7 Acetaminophen (paracetamol) 1.20 0.9548 N/A N/A N/A N/A N/A N/A 126.11 7,73 13.96 79.54 17,10 13.04 105.72 14,92 29.30
8 Acetamiprid 0.40 0.9967 N/A N/A N/A 113.51 14,76 3.73 97.67 11,75 2.41 104.22 17,94 4.72 95.95 7,89 1.24
9 Acrinathrin 1.20 0.9943 N/A N/A N/A N/A N/A N/A 109.46 9,36 10.87 93.81 6,62 5.87 99.70 16,60 9.75
10 Albendazole 0.10 0.9952 121.06 10,61 8.38 96.22 9,08 10.63 99.00 10,54 1.33 108.29 17,77 3.44 96.38 14,56 0.81
11 Aldicarb 0.10 0.9956 118.27 18,28 14.53 98.52 10,06 4.99 92.82 8,85 1.70 102.55 6,62 5.28 95.35 13,66 3.09
12 Aldicarb-sulfone 0.40 0.9966 N/A N/A N/A 118.79 12,30 5.58 93.35 10,83 7.71 99.82 6,62 4.56 96.53 7,31 1.87
13 Aldicarb-sulfoxide 1.60 0.9936 N/A N/A N/A N/A N/A N/A N/A N/A N/A 100.26 6,62 1.11 94.55 7,50 0.14
14 Aldrin 0.40 0.9951 N/A N/A N/A 95.34 15,89 4.08 97.07 13,35 9.52 95.19 6,86 0.34 97.66 7,25 1.76
15 Anthracene 0.80 0.9579 N/A N/A N/A N/A N/A N/A 114.90 7,72 6.49 92.78 14,13 9.89 95.94 14,59 8.63
16 Atrazine 0.10 0.9960 107.95 8,69 1.74 97.69 16,36 17.22 93.12 13,51 3.34 103.37 15,25 5.44 95.62 8,06 0.71
17 Azinphos-methyl 0.20 0.9961 N/A N/A N/A 108.57 8,99 1.85 95.64 10,75 3.62 107.13 15,31 3.49 94.57 13,68 0.15
18 Azoxystrobin 0.10 0.9972 103.13 15,68 1.38 96.51 8,98 17.06 97.09 10,29 4.55 104.23 17,56 7.15 97.49 15,71 4.20
19 BDE-28 0.20 0.9932 N/A N/A N/A 103.43 8,92 12.34 101.66 8,32 5.74 90.52 6,73 9.65 90.60 17,40 8.15
20 BDE-47 0.20 0.9924 N/A N/A N/A 96.70 15,12 7.67 100.78 11,76 5.69 91.21 17,86 9.72 94.25 8,12 8.48
21 BDE-85 0.10 0.9954 129.76 10,28 5.15 91.22 13,95 11.00 101.98 12,44 5.76 86.00 7,35 9.16 99.65 7,39 8.96
22 BDE-99 0.10 0.9934 91.23 5,37 4.22 105.76 14,85 14.54 103.28 13,00 5.83 94.33 6,64 10.05 94.77 7,85 8.52
23 BDE-100 0.10 0.9873 109.21 8,67 7.98 89.95 10,40 11.20 101.34 10,20 5.72 92.07 6,78 9.81 85.36 16,69 7.68
24 BDE-153 0.20 0.9951 N/A N/A N/A 86.36 13,46 10.95 102.38 10,65 5.78 98.11 6,62 10.45 95.42 7,26 8.58
25 BDE-154 0.10 0.9954 111.23 7,50 8.20 109.41 9,31 11.22 101.80 8,92 5.75 94.84 15,34 10.11 91.95 15,43 8.27
26 BDE-183 0.20 0.9815 N/A N/A N/A 98.77 10,04 7.64 103.39 8,47 5.84 98.97 14,04 10.55 103.42 15,38 9.30
27 Benalaxyl 0.10 0.9978 97.07 10,61 4.88 91.75 10,74 5.04 96.40 9,17 0.54 102.02 17,93 2.34 98.23 14,16 2.16
28 Bendiocarb 0.10 0.9961 106.43 17,38 11.19 98.54 16,51 11.11 88.59 11,92 0.30 101.12 17,69 7.81 95.22 7,38 1.33
29 Bendiocarb metabolite (2. 2‐dimethylbenzo‐1. 3‐dioxol‐4‐ol) 1.20 0.9968 N/A N/A N/A N/A N/A N/A 100.90 12,67 0.91 82.48 6,69 8.04 99.56 13,52 3.43
30 Benfuracarb 0.10 0.9950 86.06 8,05 10.19 103.65 14,71 15.73 99.20 13,07 2.80 106.49 13,63 4.43 95.72 14,04 5.01
31 Benzo[a]anthracene 0.80 0.9805 N/A N/A N/A N/A N/A N/A 111.54 7,78 6.30 94.91 6,69 10.11 89.36 9,08 8.04
32 Benzo[a]pyrene 0.10 0.9948 124.45 14,20 9.32 95.76 14,39 6.53 112.23 10,04 6.34 95.02 6,67 10.13 101.13 12,65 9.09
33 Benzo[b]fluoranthene 0.80 0.9766 N/A N/A N/A N/A N/A N/A 105.05 8,54 5.93 92.65 6,62 9.87 98.55 10,27 8.86
34 Benzo[ghi]perylene 0.40 0.9912 N/A N/A N/A 119.14 9,12 7.22 111.18 12,61 6.28 99.29 6,67 10.58 103.47 9,06 9.30
35 Benzo[k]fluoranthene 0.40 0.9323 N/A N/A N/A 95.12 9,17 9.12 95.35 15,14 5.39 100.05 16,54 10.66 94.17 10,62 8.47
36 Bifenthrin 0.20 0.9952 N/A N/A N/A 98.48 13,53 12.82 102.14 10,00 1.84 89.51 18,10 3.56 95.27 13,67 5.57
37 Bitertanol 0.40 0.9938 N/A N/A N/A 105.62 14,27 15.92 105.68 9,81 13.20 102.68 10,19 5.54 96.23 14,00 7.53
38 Boscalid (formerly nicobifen) 0.10 0.9974 112.80 9,55 7.39 101.63 14,86 4.10 97.54 10,08 6.17 84.80 10,06 7.47 100.58 12,54 5.73
39 Brodifacoum 0.80 0.9806 N/A N/A N/A N/A N/A N/A 92.73 13,12 5.11 96.45 15,56 15.43 100.49 9,93 12.33
40 Bromadiolone 0.40 0.9864 N/A N/A N/A 116.06 10,17 18.62 89.90 9,56 5.46 112.93 9,46 3.98 100.80 16,46 0.11
41 Bromopropylate 0.20 0.9887 N/A N/A N/A 99.38 14,28 11.80 102.94 12,91 14.65 88.10 13,47 2.10 98.29 9,89 17.90
42 Bromuconazole (two isomers) 0.20 0.9821 N/A N/A N/A 97.91 12,92 8.33 98.52 13,61 11.16 87.58 14,54 19.50 99.45 9,70 9.08
43 Bupirimate 0.20 0.9940 N/A N/A N/A 97.15 13,95 10.65 97.41 12,47 1.67 88.40 9,36 2.98 97.21 10,00 5.20
44 Buprofezin 0.10 0.9930 111.89 12,12 7.55 93.70 10,78 4.48 91.32 8,97 3.26 96.80 11,53 3.61 97.21 15,68 7.98
45 Cadusafos (ebufos) 0.10 0.9956 86.62 9,70 9.96 94.38 9,34 11.50 103.53 9,81 5.16 105.85 13,64 4.40 95.85 15,07 2.52
46 Carbaryl 0.10 0.9978 106.07 9,25 5.31 94.48 9,87 3.35 98.38 10,04 9.69 105.00 13,67 4.09 96.64 14,97 3.48
47 Carbendazim (azole) 0.40 0.9965 N/A N/A N/A 118.80 13,28 3.68 94.83 13,87 3.95 101.66 13,34 4.74 97.47 9,11 2.27
48 Carbofuran 0.10 0.9959 118.09 12,71 9.84 93.02 11,68 15.57 90.26 9,61 3.87 98.83 12,60 9.04 96.21 14,66 4.67
49 Carbofuran-3-hydroxy 0.40 0.9963 N/A N/A N/A 117.69 12,90 6.37 96.99 13,89 4.38 103.10 13,92 4.90 95.70 9,44 2.86
50 Carbosulfan 0.40 0.9781 N/A N/A N/A 132.53 12,51 5.32 84.83 13,15 18.63 110.47 9,64 9.70 105.49 9,25 3.40
51 Cefuroxima axetil (two isomers) 0.80 0.9902 N/A N/A N/A N/A N/A N/A 105.25 14,44 3.61 100.04 10,23 5.53 104.99 8,89 2.88
52 Chloramphenicol 2.00 0.9814 N/A N/A N/A N/A N/A N/A N/A N/A N/A 120.55 9,33 11.01 102.82 12,43 9.86
53 Chlorantraniliprole 0.20 0.9952 N/A N/A N/A 107.14 9,74 13.70 91.93 9,32 10.91 104.44 9,61 6.25 95.70 13,94 4.00
54 Chlorfenapyr 1.20 0.9936 N/A N/A N/A N/A N/A N/A 97.07 8,89 12.36 85.57 13,88 11.55 106.01 14,26 1.61
55 Chlorfenvinphos 0.20 0.9969 N/A N/A N/A 96.71 14,12 11.93 100.05 14,95 5.73 102.06 9,37 0.48 96.97 9,73 0.29
56 Chlorobenzilate 0.40 0.9909 N/A N/A N/A 88.96 9,99 9.32 105.63 8,87 5.97 87.66 15,64 9.34 89.59 14,82 8.06
57 Chlorophacinone 0.80 0.9874 N/A N/A N/A N/A N/A N/A 96.82 12,73 1.94 103.81 13,52 2.08 100.62 9,72 4.45
58 Chlorpropham 0.20 0.9949 N/A N/A N/A 110.12 13,64 10.89 101.16 13,17 9.22 85.27 16,60 9.82 97.24 10,40 9.23
59 Chlorpyrifos 0.80 0.9915 N/A N/A N/A N/A N/A N/A 100.64 14,14 10.32 91.52 15,69 7.57 100.79 10,24 7.46
60 Chlorpyrifos methyl 0.40 0.9951 N/A N/A N/A 103.73 9,45 7.79 104.81 9,61 13.90 88.99 10,69 10.67 99.45 13,30 4.76
61 Chlorthal dimethyl 0.20 0.9874 N/A N/A N/A 91.40 11,74 4.48 107.91 8,89 7.07 90.69 9,27 3.38 96.20 14,69 7.87
62 Chrysene 0.80 0.9789 N/A N/A N/A N/A N/A N/A 109.29 9,22 6.17 93.19 9,29 9.93 94.31 13,57 8.48
63 Clindamycin 0.40 0.9970 N/A N/A N/A 116.37 11,77 4.52 96.24 12,64 9.31 104.48 10,53 6.42 97.59 9,89 1.83
64 Clofentezine 0.40 0.9944 N/A N/A N/A 101.79 9,49 2.24 96.83 9,70 1.32 107.77 13,16 5.27 98.86 14,77 0.82
65 Clothianidin 1.20 0.9941 N/A N/A N/A N/A N/A N/A 89.69 13,57 2.55 100.83 9,18 9.29 93.83 9,88 2.69
66 Cloxacillin 1.60 0.9803 N/A N/A N/A N/A N/A N/A N/A N/A N/A 110.09 14,70 3.00 101.78 9,10 3.38
67 Cortiscosterone 21 acetate 0.80 0.9948 N/A N/A N/A N/A N/A N/A 116.41 14,25 25.41 105.76 12,62 1.63 97.81 9,06 4.02
68 Coumachlor 0.20 0.9948 N/A N/A N/A 95.39 9,51 2.10 101.51 9,31 2.76 109.44 14,42 6.63 99.44 16,00 6.43
69 Coumaphos 0.10 0.9977 116.47 12,99 9.03 87.29 10,10 2.13 93.40 8,98 5.88 102.10 12,07 4.65 98.22 13,49 5.08
70 Coumatetralyl 0.40 0.9791 N/A N/A N/A 104.44 9,23 14.38 104.06 9,03 13.27 91.59 9,96 1.15 98.21 14,37 11.04
71 Cyazofamid 0.80 0.9973 N/A N/A N/A N/A N/A N/A 106.76 12,52 2.68 103.61 10,04 6.11 98.92 9,10 1.86
72 Cyflufenamid 0.20 0.9936 N/A N/A N/A 85.26 11,55 2.59 112.30 9,20 13.66 110.04 9,40 2.12 96.14 14,03 7.41
73 Cyfluthrin (sum of four isomers) 1.20 0.9923 N/A N/A N/A N/A N/A N/A 102.22 15,22 2.03 89.47 10,43 0.08 100.93 9,55 0.81
74 Cyhalothrin (lambda isomer) 2.00 0.9938 N/A N/A N/A N/A N/A N/A N/A N/A N/A 95.52 15,51 10.00 100.53 9,65 1.89
75 Cymoxanil 0.40 0.9975 N/A N/A N/A 114.66 12,65 10.00 96.84 14,55 1.40 101.03 9,71 5.35 96.68 10,08 1.83
76 Cypermethrin (sum of four isomers) 4.00 0.9886 N/A N/A N/A N/A N/A N/A N/A N/A N/A 94.85 13,60 7.83 102.11 14,45 7.39
77 Cyproconazole (two isomers) 0.40 0.9952 N/A N/A N/A 102.85 10,03 18.32 98.08 9,04 4.73 104.80 13,46 5.60 96.12 14,27 2.98
78 Cyprodinil 0.20 0.9945 N/A N/A N/A 109.65 9,34 10.35 95.04 10,01 19.09 103.39 14,24 5.60 95.75 12,78 3.91
79 Cyromazine 2.00 0.9904 N/A N/A N/A N/A N/A N/A N/A N/A N/A 97.88 15,22 0.44 101.73 10,16 2.26
80 Danofloxacin 1.20 0.9698 N/A N/A N/A N/A N/A N/A 87.87 15,46 4.73 88.06 9,23 1.32 95.42 16,22 21.72
81 Dazomet 1.60 0.9954 N/A N/A N/A N/A N/A N/A N/A N/A N/A 107.37 10,51 9.72 100.18 9,74 4.16
82 Deltamethrin 0.80 0.9927 N/A N/A N/A N/A N/A N/A 104.72 7,30 11.36 118.20 12,06 2.60 98.42 8,92 1.75
83 Demeton-S-methyl 0.10 0.9966 113.64 12,45 4.39 98.56 13,75 7.34 91.34 8,63 1.66 100.20 14,19 7.48 95.83 12,90 0.52
84 Demeton-S-methyl-sulfone (Dioxydemeton) 0.40 0.9962 N/A N/A N/A 116.45 10,04 12.58 98.84 15,84 1.65 101.43 12,71 5.48 97.04 9,37 0.23
85 Dexamethasone 0.40 0.9920 N/A N/A N/A 129.03 9,03 9.22 100.41 12,98 4.52 102.29 13,81 11.14 94.51 10,33 0.39
86 Diazinon 0.40 0.9923 N/A N/A N/A 106.32 10,31 1.65 110.27 15,60 13.64 90.53 9,96 8.70 97.56 10,05 3.30
87 Dibenzo[a.h]anthracene 0.40 0.9884 N/A N/A N/A 122.87 13,55 14.78 106.79 7,27 6.03 95.70 13,68 10.20 100.26 14,21 9.02
88 Dichlorodiphenyldichloroethane (p.p’ DDD) 0.10 0.9783 93.23 6,40 7.21 95.01 10,77 9.24 115.50 12,04 6.52 88.01 14,59 9.38 86.76 10,58 7.80
89 Dichlorodiphenyldichloroethylene (p.p’ DDE) 0.10 0.9848 94.34 8,74 5.45 95.01 15,21 7.23 115.50 7,37 6.52 88.01 13,38 9.38 86.76 15,66 7.80
90 Dichlorodiphenyltrichloroethane (p.p’ DDT) 1.20 0.9740 N/A N/A N/A N/A N/A N/A 124.05 7,26 4.15 82.09 11,36 19.34 97.14 12,26 17.84
91 Diclofenac 0.80 0.9677 N/A N/A N/A N/A N/A N/A 79.69 9,75 18.79 104.25 15,50 6.86 104.76 14,33 0.55
92 Dicloran 0.10 0.9836 123.22 9,55 8.22 108.31 9,22 11.23 114.09 14,60 6.44 107.57 9,01 11.46 99.19 9,49 8.92
93 Dicloxacillin 1.20 0.9832 N/A N/A N/A N/A N/A N/A 118.47 13,71 25.92 107.63 9,22 2.05 94.46 11,45 8.19
94 Dieldrin 1.20 0.9916 N/A N/A N/A N/A N/A N/A 90.79 16,01 2.75 93.04 10,08 18.65 102.23 10,10 6.68
95 Diethathyl ethyl 0.20 0.9949 N/A N/A N/A 101.03 13,95 15.93 97.12 8,14 6.24 109.86 9,80 1.29 97.92 13,74 5.33
96 Diethofencarb 0.10 0.9974 109.28 9,41 9.22 99.69 10,24 14.33 90.50 16,03 5.04 103.94 14,12 11.39 97.29 9,31 3.12
97 Difenacoum 0.20 0.9821 N/A N/A N/A 106.25 12,62 0.67 97.13 7,96 1.76 89.59 15,15 10.58 101.79 12,53 13.24
98 Difenoconazole 0.40 0.9962 N/A N/A N/A 110.55 14,29 2.18 97.28 7,66 6.95 103.07 15,99 5.52 98.83 15,16 3.65
99 Difethialone 0.80 0.9710 N/A N/A N/A N/A N/A N/A 95.73 7,39 17.88 91.34 16,61 15.31 102.52 12,84 22.89
100 Difloxacin 0.80 0.9702 N/A N/A N/A N/A N/A N/A 74.73 16,49 11.56 95.04 9,89 3.47 97.27 10,00 24.41
101 Diflubenzuron 1.20 0.9909 N/A N/A N/A N/A N/A N/A 82.74 13,96 13.97 104.38 14,08 2.84 97.93 9,13 8.15
102 Diflufenican 0.10 0.9943 104.94 10,18 11.58 95.70 10,05 10.45 85.39 14,12 4.30 110.99 9,10 5.78 99.81 9,32 0.67
103 Dimethenamid-P (and its R-isomer) 0.10 0.9963 127.37 6,66 4.97 101.55 13,43 3.07 91.45 8,20 11.35 91.32 9,36 16.95 96.98 14,60 0.53
104 Dimethoate 0.40 0.9967 N/A N/A N/A 122.10 9,22 0.83 98.13 15,13 4.07 102.92 10,29 6.04 97.11 11,18 0.20
105 Dimethomorph (two isomers) 0.40 0.9966 N/A N/A N/A 117.73 13,92 4.31 97.14 8,28 2.29 101.37 9,10 8.66 97.41 15,53 2.53
106 Dimethylphenylsulfamide (DMSA. metabolite of dichlofluanid) 0.80 0.9971 N/A N/A N/A N/A N/A N/A 99.37 8,54 5.30 97.54 13,42 8.62 98.06 12,18 1.27
107 Diniconazole-M 0.20 0.9972 N/A N/A N/A 110.11 12,82 18.86 86.32 9,11 8.30 103.99 14,19 10.86 98.08 14,05 0.98
108 Dinocap 0.80 0.9847 N/A N/A N/A N/A N/A N/A 90.93 15,41 5.14 102.73 15,20 10.95 95.70 9,66 8.61
109 Diphacinone 1.20 0.9892 N/A N/A N/A N/A N/A N/A 115.88 13,56 4.43 105.36 16,11 8.05 98.59 9,73 5.59
110 Diphenylamine 0.20 0.9938 N/A N/A N/A 104.56 10,04 10.33 100.70 16,33 1.21 81.45 9,71 11.19 103.06 9,82 2.82
111 Dodine 0.40 0.9953 N/A N/A N/A 98.40 15,62 11.83 102.50 8,23 1.46 101.49 12,47 2.92 95.74 15,22 2.74
112 Endosulfan alfa 0.80 0.9931 N/A N/A N/A N/A N/A N/A 101.76 12,52 13.79 86.34 9,89 13.22 100.60 9,22 2.10
113 Endosulfan beta 0.80 0.9859 N/A N/A N/A N/A N/A N/A 116.18 8,01 17.11 94.87 8,97 15.61 102.32 12,87 8.66
114 Endosulfan sulfate 0.80 0.9884 N/A N/A N/A N/A N/A N/A 111.36 7,97 4.46 99.14 10,28 12.76 101.10 13,93 4.21
115 Endrin 1.60 0.9961 N/A N/A N/A N/A N/A N/A N/A N/A N/A 105.62 8,92 11.25 83.94 14,41 7.55
116 Enrofloxacin 1.20 0.9569 N/A N/A N/A N/A N/A N/A 90.24 14,45 1.61 79.66 13,76 16.02 92.99 11,50 34.07
117 EPN 0.80 0.9873 N/A N/A N/A N/A N/A N/A 100.07 16,63 3.78 94.94 15,70 17.91 98.99 9,19 2.59
118 Epoxiconazole 0.20 0.9966 N/A N/A N/A 109.95 10,50 2.71 87.76 17,90 15.32 99.14 13,04 5.31 97.64 9,13 1.60
119 Eprinomectin 0.20 0.9878 N/A N/A N/A 121.34 13,63 9.72 99.91 7,56 12.53 112.05 8,92 1.98 106.09 11,98 0.52
120 Eritromicin 0.20 0.9967 N/A N/A N/A 105.88 10,86 6.29 96.88 16,44 3.65 103.97 9,77 6.11 96.79 10,70 3.68
121 Esfenvalerate 2.00 0.9936 N/A N/A N/A N/A N/A N/A N/A N/A N/A 96.38 10,37 3.14 96.89 13,24 5.12
122 Ethion (diethion) 0.10 0.9958 103.66 7,72 0.78 89.88 15,17 3.73 95.28 7,88 3.77 108.49 8,87 4.58 100.49 15,28 4.16
123 Ethirimol 0.40 0.9964 N/A N/A N/A 122.23 12,67 1.90 96.57 12,01 0.27 104.84 12,91 3.65 98.37 13,21 4.56
124 Ethofumesate 0.80 0.9846 N/A N/A N/A N/A N/A N/A 91.55 10,20 4.97 82.64 18,27 14.03 98.52 10,25 11.95
125 Ethoprophos 0.20 0.9953 N/A N/A N/A 96.56 9,60 16.85 96.29 10,50 4.92 102.00 14,06 7.17 95.03 11,29 2.62
126 Etofenprox 0.80 0.9963 N/A N/A N/A N/A N/A N/A 98.75 10,23 4.30 93.90 15,00 7.98 100.65 9,10 5.37
127 Etoxazole 0.10 0.9972 106.66 6,86 18.17 87.77 16,23 9.12 91.35 9,95 7.34 103.72 9,01 3.18 100.75 13,94 4.65
128 Famoxadone 1.20 0.9942 N/A N/A N/A N/A N/A N/A 109.69 9,40 14.42 101.73 12,93 9.40 98.87 10,38 3.93
129 Fenamidone 0.10 0.9976 100.84 9,44 2.17 102.38 12,60 9.41 99.89 9,41 9.34 105.57 9,85 4.55 97.86 13,99 2.26
130 Fenamiphos 0.10 0.9976 92.87 15,36 1.25 94.57 14,70 9.17 99.28 8,99 1.65 107.18 9,85 5.85 95.32 13,62 3.93
131 Fenamiphos sulfone 0.20 0.9971 N/A N/A N/A 109.57 13,30 6.60 90.42 10,49 0.60 103.95 8,98 7.13 96.59 15,51 1.85
132 Fenamiphos sulfoxide 0.40 0.9963 N/A N/A N/A 120.76 9,74 4.40 96.93 9,25 3.43 99.10 9,42 7.16 97.96 10,91 0.25
133 Fenarimol 0.20 0.9960 N/A N/A N/A 107.08 10,55 8.23 100.38 7,97 1.42 91.15 14,84 3.62 98.31 9,95 0.95
134 Fenazaquin 0.80 0.9967 N/A N/A N/A N/A N/A N/A 103.00 7,70 4.49 107.95 15,93 4.82 99.17 17,83 1.81
135 Fenbendazole 0.10 0.9959 117.39 10,22 0.85 96.83 15,21 7.43 92.86 10,50 12.54 111.90 15,15 3.55 96.47 6,84 0.78
136 Fenbuconazole 0.40 0.9943 N/A N/A N/A 106.97 10,09 11.96 97.78 8,02 4.11 82.91 16,31 2.82 96.67 17,54 4.23
137 Fenbutatin oxide 0.80 0.9705 N/A N/A N/A N/A N/A N/A 101.12 10,91 2.09 101.73 10,08 2.23 109.08 6,62 3.83
138 Fenhexamid 1.60 0.9952 N/A N/A N/A N/A N/A N/A N/A N/A N/A 94.50 12,93 5.93 100.97 6,91 1.63
139 Fenitrothion 0.20 0.9946 N/A N/A N/A 96.00 13,47 1.84 104.50 10,63 18.04 89.65 10,40 10.92 98.77 6,63 0.21
140 Fenoxycarb 0.10 0.9950 106.29 15,35 14.48 89.97 9,71 10.85 88.98 8,95 0.61 108.29 14,13 1.92 101.10 17,34 1.20
141 Fenpropathrin 0.40 0.9932 N/A N/A N/A 96.77 9,48 4.11 108.60 7,36 7.89 114.09 15,57 4.22 98.64 14,32 2.46
142 Fenpropidin 0.10 0.9971 107.57 7,02 6.44 95.01 9,25 14.96 95.57 8,20 6.27 104.76 14,60 3.69 98.78 16,42 2.87
143 Fenpropimorph 0.10 0.9967 112.10 6,69 5.06 91.37 15,36 6.27 98.02 11,73 3.30 105.01 7,29 4.62 98.31 7,08 2.04
144 Fenpyroximate 0.40 0.9972 N/A N/A N/A 108.10 9,24 11.74 98.03 9,60 3.42 110.63 7,30 7.96 99.89 14,81 3.51
145 Fenthion 0.10 0.9907 101.39 8,20 9.98 98.48 14,20 6.59 100.84 10,07 1.09 93.69 7,24 3.06 97.74 6,90 2.60
146 Fenthion oxon 0.10 0.9981 102.81 9,49 11.00 93.65 12,81 5.77 95.62 9,66 2.50 103.73 7,29 4.97 97.83 6,63 1.80
147 Fenthion oxon sulfone 0.80 0.9978 N/A N/A N/A N/A N/A N/A 99.68 9,78 2.02 101.55 16,22 6.88 98.19 6,93 2.88
148 Fenthion oxon sulfoxide 0.20 0.9977 N/A N/A N/A 119.70 9,46 1.24 99.13 9,09 5.16 101.41 7,40 5.89 97.91 18,80 0.84
149 Fenthion sulfone 0.80 0.9980 N/A N/A N/A N/A N/A N/A 102.66 8,33 0.50 101.78 13,19 9.01 98.32 17,66 2.07
150 Fenthion sulfoxide 0.40 0.9991 N/A N/A N/A 106.77 10,32 6.95 103.30 9,24 8.77 103.57 16,11 4.88 95.47 15,28 1.90
151 Fenvalerate 2.00 0.9939 N/A N/A N/A N/A N/A N/A N/A N/A N/A 91.05 15,63 10.82 98.09 6,62 1.48
152 Fipronil 0.20 0.9946 N/A N/A N/A 104.05 9,16 2.31 90.35 10,22 2.29 101.81 13,15 4.10 100.66 15,46 0.15
153 Fipronil sulfide 0.80 0.9391 N/A N/A N/A N/A N/A N/A 98.90 11,00 8.97 84.35 7,92 13.73 95.07 7,23 27.31
154 Flocoumafen 0.20 0.9737 N/A N/A N/A 115.03 13,55 2.97 97.42 10,83 10.78 81.77 8,58 6.71 99.46 6,62 19.13
155 Fluazinam 0.20 0.9942 N/A N/A N/A 109.04 13,34 9.01 95.48 10,76 4.20 101.92 7,31 1.50 96.92 6,62 2.29
156 Flubendiamide 2.00 0.9829 N/A N/A N/A N/A N/A N/A N/A N/A N/A 91.98 8,33 10.12 95.45 17,55 9.10
157 Flucythrinate (two isomers) 0.80 0.9951 N/A N/A N/A N/A N/A N/A 100.00 9,93 2.37 93.42 16,52 4.71 99.66 14,19 4.20
158 Fludioxonil 0.20 0.9924 N/A N/A N/A 99.12 9,56 6.85 96.89 9,31 6.19 88.02 7,25 3.14 98.96 17,89 9.67
159 Flufenoxuron 0.10 0.9942 107.97 6,05 14.68 88.19 14,34 10.25 88.31 12,00 4.19 112.03 7,62 4.34 102.01 6,75 2.92
160 Flumequine 0.10 0.9876 106.13 8,91 23.04 100.69 11,01 10.95 91.44 8,68 9.51 96.97 9,32 10.04 91.89 15,61 17.35
161 Flunixin 0.20 0.9949 N/A N/A N/A 96.90 14,66 4.63 91.59 9,37 1.62 110.14 7,43 2.78 98.17 6,63 0.65
162 Fluopyram 0.20 0.9958 N/A N/A N/A 110.51 12,65 3.31 97.01 11,93 0.48 94.66 9,95 8.92 96.17 6,77 6.46
163 Fluoranthene 0.20 0.9887 N/A N/A N/A 109.74 13,17 6.76 104.20 11,02 5.89 94.00 7,25 10.02 85.54 7,48 7.69
164 Fluorene 0.20 0.9836 N/A N/A N/A 148.49 9,00 13.22 111.31 8,80 6.29 92.49 16,86 9.86 93.39 17,74 8.40
165 Fluquinconazole 0.20 0.9869 N/A N/A N/A 103.74 10,15 12.58 96.88 8,10 4.65 88.44 17,22 1.18 96.68 17,03 13.29
166 Flusilazole 0.20 0.9946 N/A N/A N/A 94.54 9,43 10.00 89.82 10,64 0.48 114.38 15,47 2.02 98.57 14,14 2.32
167 Flutolanil 0.10 0.9975 106.84 7,89 11.91 89.48 13,65 6.56 100.18 11,64 5.67 106.33 16,01 3.74 98.51 6,62 2.19
168 Flutriafol 0.20 0.9953 N/A N/A N/A 96.42 10,14 7.37 105.15 9,45 8.63 90.02 8,07 2.90 96.88 17,53 0.89
169 Fluvalinate tau 4.00 0.9356 N/A N/A N/A N/A N/A N/A N/A N/A N/A 90.97 7,25 5.31 106.96 6,69 10.74
170 Fonofos 0.40 0.9924 N/A N/A N/A 104.18 13,29 14.80 101.25 11,79 6.87 87.63 7,29 10.09 97.22 6,69 4.61
171 Formetanate 0.10 0.9967 106.33 13,02 9.84 96.75 14,29 0.48 94.60 10,34 0.85 109.06 7,56 4.34 100.01 6,95 5.73
172 Fosthiazate 0.10 0.9972 106.58 11,43 10.48 97.01 9,22 10.28 95.35 8,80 6.45 101.87 15,78 5.69 96.64 14,66 1.77
173 Heptachlor 0.80 0.9722 N/A N/A N/A N/A N/A N/A 87.12 8,39 4.92 139.37 7,28 14.85 92.22 14,83 8.29
174 Hexachlorobencene 0.20 0.9858 N/A N/A N/A 99.79 9,37 9.45 105.21 8,36 5.94 93.97 16,62 10.01 93.24 15,11 8.38
175 Hexachlorocyclohexane (alpha) 0.40 0.9818 N/A N/A N/A N/A N/A N/A 104.74 10,64 5.92 104.70 13,30 11.16 102.65 6,65 9.23
176 Hexachlorocyclohexane (beta) 0.40 0.9456 N/A N/A N/A N/A N/A N/A 113.08 7,52 6.39 132.60 13,78 14.13 109.11 14,55 9.81
177 Hexachlorocyclohexane (delta) 0.20 0.9803 N/A N/A N/A 78.98 14,62 7.89 103.75 10,97 5.86 108.30 13,54 11.54 100.42 6,69 9.03
178 Hexaclorocyclohexane (gamma. lindane) 1.20 0.9788 N/A N/A N/A N/A N/A N/A 74.44 10,23 4.20 116.82 7,46 12.45 109.76 6,66 9.87
179 Hexaconazole (two isomers) 0.80 0.9956 N/A N/A N/A N/A N/A N/A 102.27 13,88 4.57 99.87 7,28 3.77 100.02 6,65 4.07
180 Hexaflumuron 0.40 0.9942 N/A N/A N/A 108.89 9,42 12.82 90.01 9,26 4.34 105.96 7,25 4.78 101.95 16,19 1.84
181 Hexythiazox 0.10 0.9901 100.56 8,48 12.26 92.79 9,89 0.73 88.30 9,01 12.34 108.98 7,31 4.58 101.78 15,67 2.78
182 Imazalil (enilconazole) 0.40 0.9962 N/A N/A N/A 109.11 10,51 1.10 99.07 9,60 0.11 105.22 14,79 1.79 100.07 17,30 5.52
183 Imidacloprid 0.80 0.9952 N/A N/A N/A N/A N/A N/A 87.81 15,08 2.99 104.63 7,28 11.64 96.04 6,63 2.58
184 Indeno [1.2.3-cd] pyrene 0.40 0.9919 N/A N/A N/A N/A N/A N/A 104.74 9,05 5.92 104.70 13,91 11.16 102.65 15,55 9.23
185 Indoxacarb 0.20 0.9936 N/A N/A N/A 107.04 14,47 9.81 90.81 17,33 0.63 104.94 16,20 0.90 100.08 6,69 2.82
186 Iprodione 4.00 0.9910 N/A N/A N/A N/A N/A N/A N/A N/A N/A 92.28 16,39 18.00 99.85 6,62 5.16
187 Iprovalicarb 0.20 0.9976 N/A N/A N/A 104.86 13,80 1.64 96.91 14,24 4.68 104.31 6,64 5.23 99.02 7,01 2.18
188 Isocarbophos 1.60 0.9921 N/A N/A N/A N/A N/A N/A N/A N/A N/A 97.94 14,54 9.86 101.76 14,94 7.87
189 Isofenphos methyl 0.40 0.9915 N/A N/A N/A 109.93 9,31 13.09 103.10 9,03 4.81 90.82 16,19 8.17 97.95 17,33 9.64
190 Isoprothiolane 0.10 0.9964 116.56 8,05 1.22 88.49 11,32 14.49 97.12 9,55 1.20 104.61 17,73 4.03 98.25 16,45 3.16
191 Ivermectin B1a 1.60 0.9537 N/A N/A N/A N/A N/A N/A N/A N/A N/A 105.65 17,48 10.35 105.44 6,85 17.66
192 Josamycin 0.40 0.9963 N/A N/A N/A 116.58 9,84 9.00 103.29 9,03 8.32 100.89 6,75 3.99 97.02 14,41 4.09
193 Ketoprofen 0.40 0.9947 N/A N/A N/A 111.09 13,69 9.48 91.37 15,03 5.33 104.97 16,90 2.64 95.12 6,88 4.68
194 Kresoxim methyl 1.20 0.9954 N/A N/A N/A N/A N/A N/A 102.98 15,93 5.45 88.44 6,70 7.22 96.75 6,67 3.56
195 Leptophos 0.80 0.9941 N/A N/A N/A N/A N/A N/A 101.99 16,06 1.71 98.45 6,98 9.13 98.20 6,83 6.65
196 Levamisole 0.20 0.9928 N/A N/A N/A 117.03 9,11 15.55 93.61 9,12 5.55 101.49 6,99 1.47 94.01 15,02 3.40
197 Lincomycin 0.40 0.9954 N/A N/A N/A 107.94 10,04 20.27 92.20 9,04 10.96 106.37 6,74 7.35 97.78 16,09 7.36
198 Linuron 0.20 0.9950 N/A N/A N/A 111.70 9,18 8.45 96.83 9,31 11.03 104.59 17,99 2.83 97.46 13,85 1.94
199 Lufenuron 0.40 0.9451 N/A N/A N/A 124.88 12,48 1.73 104.02 14,96 4.07 76.66 19,41 9.50 108.83 6,75 6.81
200 Malaoxon 0.10 0.9968 105.72 13,29 7.33 98.47 10,73 10.38 93.12 9,21 5.62 103.41 6,91 5.54 96.61 13,88 1.87
201 Malathion 0.20 0.9956 N/A N/A N/A 102.68 15,17 2.06 108.09 15,52 6.64 108.81 6,62 6.47 95.13 6,74 1.66
202 Mandipropamid 0.10 0.9965 115.12 12,98 1.19 88.72 12,74 4.12 94.24 16,17 0.83 104.13 6,65 1.48 97.38 6,62 1.67
203 Marbofloxacin 2.00 0.9589 N/A N/A N/A N/A N/A N/A N/A N/A N/A 58.20 8,81 13.63 95.33 6,67 21.85
204 Mebendazole 0.10 0.9960 139.72 14,34 0.62 93.53 9,81 2.13 93.17 9,63 5.68 104.77 16,51 3.77 97.25 14,46 2.70
205 Mefenamic acid 0.40 0.9938 N/A N/A N/A 111.93 10,36 4.50 97.29 9,33 11.22 106.39 15,98 0.91 101.74 16,63 0.41
206 Mefenoxam (metalaxyl-M) 0.10 0.9974 104.72 14,28 6.08 101.99 9,15 10.56 95.87 9,02 4.94 103.12 15,00 7.93 96.94 15,42 2.84
207 Meloxicam 0.20 0.9916 N/A N/A N/A 105.76 13,99 8.34 103.10 16,06 8.66 103.87 15,74 0.35 95.21 6,62 7.62
208 Mepanipyrim 0.40 0.9940 N/A N/A N/A 112.41 9,22 16.49 100.23 9,21 5.60 86.88 7,31 4.08 98.52 18,16 5.19
209 Mepiquat 0.40 0.9961 N/A N/A N/A 116.63 13,85 16.83 102.27 15,30 6.19 109.64 15,10 6.19 98.75 6,68 1.89
210 Metaflumizone 0.20 0.9538 N/A N/A N/A 117.95 13,04 7.80 110.07 14,54 14.54 78.67 7,94 1.92 108.66 7,10 15.31
211 Metaldehyde 4.00 0.9883 N/A N/A N/A N/A N/A N/A N/A N/A N/A 93.85 6,69 11.49 99.36 7,06 5.12
212 Metconazole 0.10 0.9972 112.89 17,30 7.83 90.40 10,89 3.31 94.39 9,51 3.75 106.51 6,73 5.49 99.30 7,31 1.11
213 Methamidophos (two isomers) 1.20 0.9914 N/A N/A N/A N/A N/A N/A 106.70 9,02 11.46 118.60 6,73 4.89 100.44 7,26 3.27
214 Methidathion 0.10 0.9971 103.57 9,74 14.60 93.56 11,22 7.71 97.65 9,08 0.47 105.01 15,31 4.15 98.65 7,31 3.48
215 Methiocarb 0.10 0.9988 102.06 8,49 8.48 80.51 15,96 14.62 104.48 15,11 0.95 102.47 15,17 6.24 99.13 15,56 0.40
216 Methiocarb-sulfoxide 0.80 0.9983 N/A N/A N/A N/A N/A N/A 106.81 9,41 3.29 100.84 16,38 3.36 99.34 7,92 2.12
217 Methomyl 0.40 0.9957 N/A N/A N/A 123.44 12,82 2.09 97.84 14,07 5.96 103.37 18,15 3.88 97.62 16,66 3.36
218 Methomyl oxime 8.00 0.9878 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 104.43 16,22 11.23
219 Methoxyfenozide 0.10 0.9970 101.72 8,47 12.57 94.61 12,59 7.91 92.06 16,58 4.97 107.21 16,10 4.63 98.53 14,79 5.72
220 Metoxychlor 0.80 0.9654 N/A N/A N/A N/A N/A N/A 103.00 9,01 4.49 107.95 6,76 4.82 99.17 7,25 1.81
221 Metrafenone 0.10 0.9961 105.81 19,69 4.81 96.19 10,87 16.34 92.34 9,58 1.92 104.28 6,62 2.67 97.90 7,25 4.32
222 Metronidazole 0.80 0.9962 N/A N/A N/A N/A N/A N/A 98.63 9,76 3.50 102.00 6,68 8.71 95.00 7,37 3.36
223 Mevinphos (phosdrin) 0.80 0.9915 N/A N/A N/A N/A N/A N/A 107.53 13,72 1.76 101.38 6,92 3.71 96.27 16,29 4.50
224 Mirex 2.00 0.9549 N/A N/A N/A N/A N/A N/A N/A N/A N/A 94.53 15,92 10.07 80.16 9,18 7.21
225 Monocrotophos 0.80 0.9965 N/A N/A N/A N/A N/A N/A 103.97 8,42 2.26 101.05 18,14 3.31 98.38 16,59 0.70
226 Myclobutanil 0.10 0.9951 124.02 8,55 14.29 90.40 14,35 1.18 93.06 10,29 11.51 104.50 14,50 1.48 97.54 14,00 1.84
227 N-(2.4-dimethylphenyl)-N’-methylformamidine (DMPF. metabolite of amitraz) 0.80 0.9974 N/A N/A N/A N/A N/A N/A 97.86 8,07 10.59 103.78 14,78 4.26 97.74 15,81 2.58
228 N.N-dimethylformamidine (DMF. metabolite of amitraz) 1.20 0.9835 N/A N/A N/A N/A N/A N/A 100.61 13,54 3.89 89.22 6,62 8.12 94.96 7,43 5.62
229 N.N-Dimethyl-N'-p-tolylsulphamide (DMST. metabolite of tolyfluanid) 0.20 0.9972 N/A N/A N/A 103.04 10,88 5.68 93.42 10,84 1.84 103.03 16,30 5.97 96.86 7,99 1.30
230 Nafcillin 0.80 0.9937 N/A N/A N/A N/A N/A N/A 88.13 14,49 4.44 108.84 6,82 0.54 103.15 7,68 2.36
231 Naphtalene 0.80 0.9321 N/A N/A N/A N/A N/A N/A 101.12 8,54 2.09 101.73 6,83 2.23 109.08 14,76 3.83
232 Naproxen 1.60 0.9915 N/A N/A N/A N/A N/A N/A N/A N/A N/A 103.39 6,66 13.15 101.78 7,24 7.98
233 Nitenpyram 2.00 0.9983 N/A N/A N/A N/A N/A N/A N/A N/A N/A 95.74 12,88 1.32 98.39 13,54 2.80
234 Novobiocin 0.80 0.9906 N/A N/A N/A N/A N/A N/A 103.08 7,97 18.91 105.94 9,44 19.94 94.20 16,68 2.89
235 Nuarimol 0.20 0.9907 N/A N/A N/A 109.73 12,42 0.51 97.78 10,16 3.72 90.15 10,54 2.92 99.33 14,45 13.10
236 Ofurace 0.10 0.9950 116.80 13,54 2.28 101.16 9,23 4.08 92.59 10,84 1.49 103.20 9,09 6.63 96.53 7,41 0.65
237 Omethoate 0.40 0.9955 N/A N/A N/A 123.46 9,26 4.50 92.85 14,57 13.56 103.56 14,05 4.38 97.89 7,34 1.03
238 Oxadixyl 0.20 0.9968 N/A N/A N/A 104.76 9,57 3.73 95.70 11,92 0.86 103.01 13,24 5.95 95.73 7,27 2.17
239 Oxamyl 0.40 0.9963 N/A N/A N/A 121.94 12,38 6.94 100.43 9,24 6.59 100.86 15,07 1.70 97.44 13,92 1.86
240 Oxfendazole 0.10 0.9958 127.49 9,14 3.24 103.94 9,83 7.55 89.18 10,70 3.62 100.67 15,04 7.94 96.27 7,42 1.82
241 Oxolinic acid 0.20 0.9878 N/A N/A N/A 115.69 14,38 16.83 83.19 8,62 3.27 93.60 11,38 7.48 91.97 13,85 12.34
242 Oxydemeton methyl 0.40 0.9957 N/A N/A N/A 121.11 14,05 6.52 92.99 8,25 1.58 101.52 9,52 5.54 97.61 15,88 2.85
243 Oxyfluorfen 0.40 0.9951 N/A N/A N/A 111.90 12,27 10.58 104.83 9,18 6.06 89.81 11,13 8.87 97.95 15,20 6.39
244 Paclobutrazol 0.40 0.9967 N/A N/A N/A 116.18 9,54 1.19 93.47 14,62 0.60 101.83 9,58 2.63 98.88 7,40 0.81
245 Paraoxon methyl 1.60 0.9967 N/A N/A N/A N/A N/A N/A N/A N/A N/A 87.46 14,41 19.55 101.53 7,25 6.01
246 Parathion ethyl 1.20 0.9566 N/A N/A N/A N/A N/A N/A 104.49 13,49 4.82 89.57 9,37 14.20 96.19 7,67 3.90
247 Parathion methyl 0.80 0.9976 N/A N/A N/A N/A N/A N/A 108.54 9,72 8.23 92.53 12,51 19.31 100.15 13,94 12.02
248 PCB 28 0.10 0.9912 83.22 13,04 15.78 93.92 10,39 11.89 106.19 11,02 6.00 97.60 12,20 10.40 88.62 7,25 7.97
249 PCB 52 0.20 0.9902 N/A N/A N/A 104.04 15,11 10.65 98.92 8,87 5.59 92.35 15,12 9.84 93.96 13,69 8.45
250 PCB 77 0.20 0.9923 N/A N/A N/A 100.53 14,86 8.65 98.89 9,22 5.59 88.02 16,35 9.38 92.40 14,65 8.31
251 PCB 81 0.10 0.9850 110.87 13,67 12.33 81.87 13,56 7.45 115.62 7,80 6.53 91.34 9,29 9.73 89.92 14,75 8.09
252 PCB 101 0.20 0.9876 N/A N/A N/A 107.84 10,20 12.34 110.75 10,27 6.26 93.40 10,87 9.95 92.89 7,29 8.35
253 PCB 105 0.10 0.9789 118.45 12,59 4.12 103.80 9,79 9.54 107.96 10,72 6.10 94.53 9,54 10.07 80.16 7,58 7.21
254 PCB 114 0.20 0.9776 N/A N/A N/A 97.14 10,43 6.22 110.95 11,13 6.27 85.53 11,13 9.11 84.13 8,29 7.57
255 PCB 118 0.20 0.9833 N/A N/A N/A 93.43 15,84 9.87 116.88 9,41 6.60 88.80 14,30 9.46 86.10 16,14 7.74
256 PCB 123 0.40 0.9834 N/A N/A N/A 96.14 9,55 11.67 106.30 12,46 6.01 88.58 9,79 9.44 85.35 7,25 7.67
257 PCB 126 0.20 0.9789 N/A N/A N/A 108.37 12,34 12.09 106.86 8,54 6.04 90.82 15,17 9.68 79.34 11,78 7.13
258 PCB 138 0.10 0.9798 107.23 9,04 9.56 91.30 13,54 9.07 110.40 8,31 6.24 92.83 14,93 9.89 84.08 9,09 7.56
259 PCB 153 0.10 0.9766 117.78 9,83 8.73 83.70 15,17 4.97 124.77 9,02 7.05 89.77 15,53 9.57 85.65 10,85 7.70
260 PCB 156 0.20 0.9912 N/A N/A N/A 98.33 10,47 7.21 107.17 16,36 6.05 91.74 15,28 9.78 77.11 17,71 6.93
261 PCB 157 0.40 0.9789 N/A N/A N/A 93.22 10,60 6.54 107.96 15,32 6.10 91.26 9,70 9.72 79.99 15,86 7.19
262 PCB 167 0.10 0.9770 102.89 9,26 6.45 91.43 11,68 8.97 102.06 14,16 5.77 86.31 9,26 9.20 81.14 15,29 7.30
263 PCB 169 0.20 0.9758 N/A N/A N/A 109.07 12,62 11.56 107.45 9,51 6.07 86.95 10,36 9.26 90.77 9,14 8.16
264 PCB 180 0.10 0.9807 119.51 8,34 20.01 87.43 12,13 10.76 113.14 15,94 6.39 85.21 11,75 9.08 95.03 13,54 8.55
265 PCB 189 0.10 0.9723 110.12 8,68 12.45 97.91 15,11 6.22 96.96 9,32 5.48 88.62 12,49 9.44 87.18 9,24 7.84
266 Penconazole 0.40 0.9930 N/A 114.19 13,25 14.47 101.18 9,00 3.31 91.43 10,09 1.78 99.02 9,49 10.75
267 Pencycuron 0.10 0.9968 97.11 8,84 9.23 94.99 12,74 13.51 93.82 9,10 3.87 105.44 12,04 6.20 97.74 9,16 0.70
268 Pendimethalin 0.80 0.9902 N/A N/A N/A N/A N/A N/A 106.58 16,84 2.61 88.47 15,67 3.62 97.69 16,40 0.06
269 Penicillin G 2.00 0.9903 N/A N/A N/A N/A N/A N/A N/A N/A N/A 117.02 13,91 3.71 97.77 12,92 3.62
270 Penicillin V 2.00 0.9917 N/A N/A N/A N/A N/A N/A N/A N/A N/A 105.81 13,39 2.98 97.69 15,53 3.59
271 Permethrin 1.20 0.9889 N/A N/A N/A N/A N/A N/A 101.46 9,10 0.12 87.27 10,84 2.23 101.87 9,16 17.84
272 Phenanthrene 0.20 0.9678 N/A N/A N/A 109.89 10,49 13.76 106.65 16,96 6.02 92.56 10,39 9.86 95.32 14,63 8.57
273 Phenylbutazone 1.60 0.9721 N/A N/A N/A N/A N/A N/A N/A N/A N/A 113.13 9,97 6.52 65.14 12,76 6.05
274 Phosalone 0.20 0.9961 N/A N/A N/A 98.37 13,12 4.61 92.71 10,27 2.58 107.98 9,30 4.93 101.62 8,94 1.06
275 Phosmet 0.20 0.9972 N/A N/A N/A 98.92 13,74 3.15 93.00 9,82 2.84 104.52 14,39 5.06 98.67 9,58 1.56
276 Phosmet oxon 0.20 0.9993 N/A N/A N/A 95.79 10,14 7.39 102.23 14,85 5.34 102.16 9,29 5.78 99.08 15,44 1.95
277 Piperacillin 0.40 0.9793 N/A N/A N/A N/A N/A N/A N/A N/A N/A 96.34 11,70 1.45 98.60 15,17 6.10
278 Pirimicarb 0.10 0.9977 105.98 8,04 2.51 98.18 10,71 6.09 95.11 15,17 5.23 102.97 10,72 4.86 97.54 15,39 1.81
279 Pirimiphos ethyl 0.10 0.9883 104.58 15,84 12.37 98.69 14,95 9.94 97.93 9,00 0.38 104.83 10,74 4.05 98.96 9,62 2.64
280 Pirimiphos methyl 0.10 0.9944 112.73 15,00 0.58 93.49 10,21 1.96 106.42 14,32 3.74 89.01 9,11 3.18 98.28 16,06 5.62
281 Prochloraz 0.10 0.9947 125.26 18,00 18.57 91.55 13,09 1.08 87.91 9,80 7.63 100.57 9,08 13.10 97.13 9,11 2.15
282 Procymidone 1.60 0.9947 N/A N/A N/A N/A N/A N/A N/A N/A N/A 80.19 15,87 6.54 100.94 9,20 5.65
283 Profenofos 0.10 0.9941 111.06 7,48 4.52 92.80 15,13 3.54 96.49 9,29 1.38 106.87 14,90 3.35 98.58 9,03 3.48
284 Propamocarb 0.40 0.9959 N/A N/A N/A 122.72 9,79 9.24 97.58 15,13 4.21 97.03 14,92 10.35 96.69 14,18 1.39
285 Propargite 0.10 0.9936 100.21 8,65 2.94 95.89 9,50 5.23 96.17 15,13 7.55 109.05 11,86 5.19 100.09 15,81 2.82
286 Propiconazole 0.40 0.9932 N/A N/A N/A 130.04 9,40 1.49 99.77 14,15 3.82 102.03 10,74 0.34 99.32 14,78 0.40
287 Propoxur 0.10 0.9941 118.68 11,02 14.25 92.88 13,46 13.27 90.94 9,34 1.25 101.89 9,97 6.43 96.39 8,93 1.71
288 Propyzamide (pronamide) 0.10 0.9955 135.09 10,13 25.43 82.62 12,64 4.33 89.32 18,24 8.08 102.57 9,70 4.21 98.22 15,95 2.04
289 Proquinazid 0.20 0.9808 N/A N/A N/A 121.75 13,90 4.37 100.38 9,85 10.36 89.96 11,39 7.16 96.95 9,40 16.39
290 Prothioconazol 0.40 0.9935 N/A N/A N/A 103.16 14,09 9.30 100.90 9,00 8.76 87.83 15,40 1.26 96.35 10,44 0.81
291 Prothiophos 0.40 0.9912 N/A N/A N/A 179.86 11,21 33.27 107.75 9,12 5.60 91.21 10,22 8.06 97.75 10,50 11.76
292 Pymetrozine 0.80 0.9952 N/A N/A N/A N/A N/A N/A 102.89 14,39 1.86 99.73 12,22 9.64 98.84 12,75 0.26
293 Pyraclostrobin 0.10 0.9970 105.05 8,46 0.95 88.71 11,51 20.65 95.80 15,56 0.93 104.40 13,96 8.09 97.82 13,51 0.60
294 Pyrazophos 0.10 0.9965 111.64 16,39 0.54 98.23 9,29 17.84 95.77 15,41 6.78 107.24 13,69 3.11 99.83 15,58 2.60
295 Pyrene 0.20 0.9880 N/A N/A N/A 96.42 13,97 9.56 93.61 9,19 5.29 93.37 13,91 9.95 91.07 9,54 8.19
296 Pyridaben 0.10 0.9973 105.99 9,65 29.54 86.82 10,63 8.41 97.27 11,31 14.36 111.71 10,40 5.14 100.32 13,91 1.83
297 Pyridaphenthion 0.20 0.9970 N/A N/A N/A 108.64 13,78 2.34 91.81 11,67 10.38 105.65 10,12 9.67 98.59 8,97 0.24
298 Pyrimethanil 0.20 0.9944 N/A N/A N/A 107.96 13,00 6.86 96.98 11,36 3.25 89.29 10,21 11.63 98.03 13,12 0.85
299 Pyriproxifen 0.10 0.9947 104.25 19,77 1.21 99.97 13,33 9.48 94.10 12,89 1.20 107.21 9,99 2.85 100.77 13,76 4.72
300 Quinalfos 0.20 0.9958 N/A N/A N/A 97.53 9,47 17.05 90.97 12,09 1.01 106.48 12,86 0.09 100.08 9,35 5.66
301 Quinoxyfen 0.10 0.9874 112.39 6,66 4.49 109.15 9,19 13.38 93.18 11,12 13.57 104.94 9,62 6.76 102.76 9,18 7.44
302 Rifampicin 0.80 0.9826 N/A N/A N/A N/A N/A N/A 111.21 10,43 10.64 95.28 14,86 0.19 89.73 11,01 5.48
303 Rotenone 0.40 0.9929 N/A N/A N/A 117.98 13,24 31.54 89.20 12,85 5.35 113.57 12,47 3.51 100.90 15,11 3.15
304 Roxithromycin 0.80 0.9971 N/A N/A N/A N/A N/A N/A 96.18 9,47 3.69 98.39 9,30 4.00 100.05 9,10 0.03
305 Sarafloxacin 4.00 0.9312 N/A N/A N/A N/A N/A N/A N/A N/A N/A 80.98 10,55 13.63 97.00 14,62 22.19
306 Simazine 0.20 0.9968 N/A N/A N/A 90.28 16,27 2.78 96.46 11,65 1.79 102.84 13,27 6.50 97.85 15,10 1.76
307 Spinosad (two isomers) 0.10 0.9970 119.58 11,44 9.10 84.56 15,73 4.96 94.98 13,13 9.89 100.78 16,05 7.72 96.81 12,98 1.95
308 Spiramycin (two isomers) 0.40 0.9915 N/A N/A N/A 131.47 9,05 5.94 95.33 9,51 14.39 106.27 13,21 4.78 97.03 10,02 3.05
309 Spirodiclofen 0.80 0.9869 N/A N/A N/A N/A N/A N/A 106.47 10,78 1.93 134.35 14,32 8.81 100.48 10,43 7.70
310 Spiromesifen 0.20 0.9911 N/A N/A N/A 96.47 9,96 13.07 101.29 9,33 5.45 115.81 8,86 4.16 100.68 10,51 2.72
311 Spiroxamine 0.10 0.9972 107.65 10,26 2.69 97.02 13,19 5.23 95.80 13,52 6.32 102.89 14,63 3.99 97.41 13,84 4.04
312 Strychnine 0.80 0.9963 N/A N/A N/A N/A N/A N/A 85.40 12,44 3.11 111.08 9,35 6.47 96.91 10,99 12.19
313 Sulfacetamide 0.40 0.9952 N/A N/A N/A 118.98 12,18 24.55 101.34 12,33 3.97 97.43 9,68 12.30 96.06 12,88 2.45
314 Sulfachloropiridacine 0.80 0.9930 N/A N/A N/A N/A N/A N/A 93.69 13,68 3.92 102.35 8,92 8.67 94.47 14,20 0.06
315 Sulfadiacine 0.80 0.9933 N/A N/A N/A N/A N/A N/A 97.95 12,68 8.67 95.92 10,00 14.59 98.24 12,94 6.24
316 Sulfadimetoxine 0.10 0.9962 122.34 7,01 0.77 104.34 9,54 10.58 94.70 10,65 12.38 103.45 15,28 9.68 96.93 10,87 1.88
317 Sulfadoxine 0.10 0.9949 129.86 7,48 12.83 92.91 9,62 4.59 92.41 10,95 6.06 104.11 12,45 8.47 95.40 9,22 4.00
318 Sulfameracine 0.20 0.9941 N/A N/A N/A 102.32 11,05 16.69 99.10 9,71 8.73 105.86 8,98 9.54 95.49 9,31 1.52
319 Sulfametacine 0.20 0.9939 N/A N/A N/A 98.96 12,83 1.51 97.49 11,61 3.97 103.52 8,92 8.64 95.26 13,20 1.45
320 Sulfametizole 0.80 0.9864 N/A N/A N/A N/A N/A N/A 100.19 10,28 0.31 103.59 8,94 10.59 91.01 9,92 3.80
321 Sulfametoxazole 0.40 0.9948 N/A N/A N/A 112.21 12,92 9.16 94.31 14,06 6.41 103.91 10,23 10.13 94.74 14,50 3.86
322 Sulfametoxipiridacine 0.40 0.9940 N/A N/A N/A 104.29 13,02 13.05 98.89 13,20 19.85 105.96 12,95 6.19 95.01 14,99 3.00
323 Sulfamonomethoxine 1.20 0.9913 N/A N/A N/A N/A N/A N/A 111.11 11,11 3.29 93.85 13,38 10.90 96.63 14,16 2.94
324 Sulfapyridine 0.40 0.9930 N/A N/A N/A 109.50 9,43 3.94 103.66 9,59 8.63 98.18 13,72 7.97 95.32 11,29 0.42
325 Sulfaquinoxaline 0.40 0.9962 N/A N/A N/A 115.47 9,35 15.86 92.67 9,83 12.76 101.15 14,97 7.60 96.86 10,75 0.16
326 Sulfatiazole 0.40 0.9922 N/A N/A N/A 109.32 10,34 18.92 87.79 11,88 0.71 96.90 9,58 11.07 96.24 9,72 1.08
327 Sulfisoxazole 0.80 0.9965 N/A N/A N/A N/A N/A N/A 93.73 12,52 5.51 101.82 14,33 5.95 95.32 14,43 1.90
328 Tebuconazole 0.80 0.9949 N/A N/A N/A N/A N/A N/A 92.08 10,26 8.58 98.28 9,74 5.09 98.61 9,22 4.53
329 Tebufenocide 0.10 0.9947 92.74 14,93 17.37 89.88 15,24 5.86 96.15 11,17 6.53 105.61 9,47 4.63 101.10 12,57 8.24
330 Tebufenpyrad 0.10 0.9950 111.56 9,92 2.79 86.18 13,25 9.05 95.86 12,29 4.97 106.62 9,27 4.29 100.57 6,66 3.07
331 Teflubenzuron 1.20 0.9860 N/A N/A N/A N/A N/A N/A 97.01 11,66 13.94 94.86 9,78 4.53 99.61 6,65 5.63
332 Tefluthrin 0.10 0.9937 97.69 9,68 14.14 104.85 10,00 3.87 107.14 10,41 2.51 88.84 15,18 4.03 95.53 14,71 1.33
333 Telodrin (isobenzan) 0.80 0.9930 N/A N/A N/A N/A N/A N/A 93.03 9,80 11.99 92.60 16,28 21.17 101.82 16,65 10.96
334 Terbufos 0.20 0.9942 N/A N/A N/A 107.98 9,37 17.24 97.29 9,28 3.06 90.31 13,69 6.42 102.47 17,11 8.75
335 Terbuthylazine 0.40 0.9961 N/A N/A N/A 98.38 12,63 4.02 93.37 14,53 2.45 91.01 13,07 11.41 99.87 6,61 3.75
336 Tetrachlorvinphos 0.40 0.9984 N/A N/A N/A 105.27 9,21 8.36 93.03 9,91 10.04 104.96 9,12 2.97 101.50 14,60 6.48
337 Tetraconazole 0.20 0.9878 N/A N/A N/A 96.23 12,80 9.69 101.26 13,96 5.09 89.84 14,01 3.49 99.52 6,84 8.62
338 Tetradifon 0.40 0.9912 N/A N/A N/A 110.62 12,25 10.72 103.75 14,09 8.41 91.10 9,45 2.57 100.16 6,91 8.47
339 Tetramethrin 1.60 0.9871 N/A N/A N/A N/A N/A N/A N/A N/A N/A 85.18 10,80 2.32 98.04 7,06 1.46
340 Thiabendazole 0.20 0.9953 N/A N/A N/A 99.82 9,60 4.72 88.38 9,69 3.77 101.10 9,07 5.74 99.15 18,69 4.46
341 Thiacloprid 0.20 0.9972 N/A N/A N/A 107.76 9,74 2.80 94.23 9,09 6.03 102.23 8,91 5.37 97.17 17,95 1.87
342 Thiamethoxam 0.80 0.9968 N/A N/A N/A N/A N/A N/A 103.40 9,05 6.94 101.22 14,16 5.43 98.61 16,69 1.97
343 Thiophanate methyl 0.20 0.9968 N/A N/A N/A 102.31 13,05 6.57 94.75 16,70 4.03 103.59 14,67 7.43 97.52 7,00 3.77
344 Tolclofos methyl 0.10 0.9922 116.17 11,56 5.73 100.20 9,86 4.71 96.78 9,59 17.32 92.67 16,21 6.45 99.05 14,51 10.76
345 Tolfenamic acid 0.40 0.9917 N/A N/A N/A 106.53 12,83 9.72 105.64 15,03 7.99 98.88 14,27 0.15 104.07 6,78 3.23
346 Triadimefon 0.40 0.9967 N/A N/A N/A 115.55 12,00 19.61 95.64 14,82 2.87 100.72 9,18 4.89 99.14 6,64 0.92
347 Triadimenol 0.40 0.9949 N/A N/A N/A 108.82 13,57 19.22 90.50 14,42 10.27 100.86 14,76 8.82 99.02 6,64 8.06
348 Triazophos (hostathion) 0.10 0.9976 97.70 9,50 9.62 97.52 9,35 2.53 96.68 9,01 10.04 103.87 9,67 4.89 98.73 17,46 3.23
349 Trichlorfon 1.20 0.9981 N/A N/A N/A N/A N/A N/A 99.76 9,02 19.77 100.02 8,98 0.34 98.66 16,06 0.59
350 Trifloxystrobin 0.10 0.9950 79.68 8,31 16.36 99.02 9,33 11.67 105.21 9,00 2.26 113.52 9,66 3.24 98.92 16,80 1.91
351 Triflumizole 0.10 0.9946 91.81 7,37 21.56 92.12 16,13 7.68 94.83 16,24 2.17 107.86 10,07 1.06 100.97 6,86 1.32
352 Triflumuron 0.40 0.9954 N/A N/A N/A 109.58 9,67 9.83 97.28 9,37 3.38 106.90 13,20 12.75 102.17 15,84 3.65
353 Trifluralin 0.20 0.9928 N/A N/A N/A 113.51 14,55 1.27 105.71 15,05 16.83 85.71 15,12 16.24 99.77 6,81 16.19
354 Trimethoprim 0.80 0.9974 N/A N/A N/A N/A N/A N/A 98.59 16,81 5.49 108.01 15,11 4.37 96.85 7,03 0.59
355 Triticonazole 0.40 0.9948 N/A N/A N/A 119.81 11,96 4.08 97.96 15,07 9.40 99.78 14,17 1.39 98.33 6,91 1.25
356 Tylmicosin 1.60 0.9955 N/A N/A N/A N/A N/A N/A N/A N/A N/A 103.10 13,68 3.57 95.24 14,57 6.28
357 Tylosin 0.80 0.9975 N/A N/A N/A N/A N/A N/A 105.10 9,03 6.25 103.84 14,83 4.75 99.16 18,48 5.44
358 Vinclozolin 0.20 0.9936 N/A N/A N/A 112.53 9,07 17.45 95.98 9,13 6.12 85.39 17,83 5.12 97.78 16,65 0.80
359 Warfarin 0.10 0.9962 106.32 9,23 20.28 90.08 13,61 15.11 92.87 16,86 4.58 103.35 13,18 3.78 98.30 6,73 0.08
360 Zoxamide 0.40 0.9960 N/A N/A N/A 126.95 9,61 10.37 94.83 9,07 3.13 101.49 12,65 5.65 98.29 15,52 1.08