. 2020 May 22;85(13):8311–8319. doi: 10.1021/acs.joc.0c01030

Table 2. Substrate Scope of the Trifluoromethylthiolation Reaction of Difluoro Enol Silyl Ethers^a.

General procedure: 2 (0.1 mmol), 3 (0.1 mmol), and KF (0.1 mmol) were stirred in MeCN (0.5 mL) at room temperature for 3 h.

¹⁹F NMR yield using PhCF₃ as the internal standard.

Reaction conducted on 1.0 mmol scale.

Table 2. Substrate Scope of the Trifluoromethylthiolation Reaction of Difluoro Enol Silyl Ethersa.