Table 3. Substrate Scope of the Trifluoromethylation Reaction of Difluoro Enol Silyl Ethersa.
General procedure: 6a (0.1 mmol), 2 (0.1 mmol), and FeCl2 (0.01 mmol) were stirred in MeCN (0.5 mL) at room temperature for 2 h.
19F NMR yield using PhCF3 as the internal standard.
With trifluoromethylbenziodoxole 6b instead.
With Umemoto reagent instead of 6a.
