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. 2020 May 22;85(13):8311–8319. doi: 10.1021/acs.joc.0c01030

Table 3. Substrate Scope of the Trifluoromethylation Reaction of Difluoro Enol Silyl Ethersa.

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a

General procedure: 6a (0.1 mmol), 2 (0.1 mmol), and FeCl2 (0.01 mmol) were stirred in MeCN (0.5 mL) at room temperature for 2 h.

b

19F NMR yield using PhCF3 as the internal standard.

c

With trifluoromethylbenziodoxole 6b instead.

d

With Umemoto reagent instead of 6a.