Table 1. Measurement parameters at the four synchrotron beamlines.
Note that total dose assumes that all frames have been included for averaging.
| Parameter | ESRF | DESY | Diamond | AustSynch |
|---|---|---|---|---|
| Detector setup | Pilatus-2M | Pilatus-6M | Eiger-4M | Pilatus-1M |
| Wavelength (nm) | 0.9919 | 1.24403 | 0.99987 | 1.07812 |
| q-Range (nm−1) | 0.0306–4.9462 | 0.0171–7.2507 | 0.0320–4.3982 | 0.0540–2.8946 |
| Sample-to-detector distance (m) | 2.849 | 3.0 | 4.014 | 2.68 |
| Per-frame exposure (s) | 0.5 | 0.1 | 2.0 | 1.0 |
| Flux at sample (photons s−1) | 5.9 × 1011 | 6.5 × 1012 | 4 × 1012 | 1.3 × 1012 |
| Total dose per frame (photons) | 3.0 × 1011 | 6.5 × 1011 | 8 × 1012 | 1.3 × 1012 |
| Frames | 10 | 40 | 20 | 20 |
| Total exposure (s) | 5 | 4 | 40 | 20 |
| Total dose (photons) | 3.0 × 1012 | 2.6 × 1013 | 1.6 × 1014 | 2.6 × 1013 |
| Average frame loss | 0 | 0 | 0 | 3 |
| Sample volume (µl) | 50 | 50 | 50 | 85 |
| Sample temperature (°C) | 20 | 20 | 20 | 20 |