Table 1. Data-collection and refinement statistics for the structure determination of RsbV–RsbW.
Values in parentheses are for the highest resolution shell.
| Monoclinic RsbV–RsbW | Hexagonal RsbV–RsbW | |
|---|---|---|
| Data collection | ||
| X-ray source | PLS II-BL11C | PLS II-BL11C |
| Space group | P21 | P6222 |
| a, b, c (Å) | 117.23, 70.94, 137.68 | 158.20, 158.20, 96.60 |
| α, β, γ (°) | 90.00, 105.35, 90.00 | 90.00, 90.00, 120.00 |
| Resolution (Å) | 50.0–3.40 (3.61–3.40) | 50.0–3.10 (3.31–3.10) |
| Wavelength (Å) | 0.97933 | 0.97933 |
| Total/unique reflections | 91522/29346 (13674/4589) | 127495/13426 (22682/2377) |
| Completeness (%) | 96.7 (94.7) | 99.9 (100.0) |
| 〈I/σ(I)〉 | 6.8 (2.4) | 15.3 (3.6) |
| R merge (%) | 14.7 (49.2) | 9.0 (65.4) |
| Refinement | ||
| Resolution (Å) | 30.0–3.40 | 50.0–3.10 |
| No. of reflections | ||
| Working | 27753 | 12750 |
| Free | 1465 | 653 |
| R work/R free (%) | 20.8/29.0 | 22.1/24.9 |
| No. of atoms | 12580 | 3330 |
| R.m.s.d. | ||
| Bond lengths (Å) | 0.011 | 0.011 |
| Bond angles (°) | 1.447 | 1.428 |
| Ramachandran plot (%) | ||
| Favored | 96.0 | 96.6 |
| Allowed | 3.8 | 2.9 |
| Disallowed | 0.2 | 0.5 |