Table 3.
Synthesis Conditions | Precursor | Elemental Analysis | XPS | |||||||
---|---|---|---|---|---|---|---|---|---|---|
Atomic Composition | C/N | N/C | C/H | Theoretic Formula | C/N | Theoretic Formula | ||||
N (at.%) | C (at.%) | H (at.%) | ||||||||
10/550/4 | D | 46.42 | 31.86 | 21.71 | 0.686 | 1.457 | 1.467 | C3N4.4H2.0 | 0.688 | C3N4.4 |
2/600/4 | D | 46.65 | 32.42 | 20.94 | 0.695 | 1.439 | 1.548 | C3N4.3H1.9 | 0.708 | C3N4.2 |
10/600/0 | D | 47.01 | 32.65 | 20.33 | 0.695 | 1.440 | 1.606 | C3N4.3H1.9 | 0.712 | C3N4.2 |
10/600/4 | D | 47.32 | 33.08 | 19.60 | 0.699 | 1.431 | 1.688 | C3N4.3H1.8 | 0.702 | C3N4.3 |
T | 46.54 | 32.33 | 21.13 | 0.695 | 1.440 | 1.530 | C3N4.3H2.0 | 0.674 | C3N4.4 | |
M | 47.46 | 33.05 | 19.48 | 0.696 | 1.436 | 1.697 | C3N4.3H1.8 | 0.687 | C3N4.4 |