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. 2020 May 26;18(6):281. doi: 10.3390/md18060281

Table 1.

1H NMR (600 MHz) and 13C NMR (150 MHz) data of compound 1 (CD3CN).

No. 1
δH, mult (J in Hz) δC
1 - 213.2
2 - 56.4
3 2.32, d (10.0) 54.8
4 - 133.2
5 5.25, br s 128.0
6 1.84, m 37.7
7 eq 1.82, m 42.9
ax 0.75, q (11.9)
8 1.44, m 33.5
9 eq 1.71, m 36.0
ax 0.83, dq (2.7, 12.6)
10 eq 1.29, dq (12.9, 3.0) 25.8
ax 1.02, m
11 1.48, ddd (11.8, 10.5, 2.7) 37.9
12 0.88, s 14.2
13 2.67, dd (10.1, 3.4) 57.0
14 4.90, dt (9.3, 3.3) 83.7
15 a 2.70, dd (16.2, 3.1) 50.3
b 2.52, dd (16.2, 9.4)
16 - 206.8
17 2.09, s 30.8
18 1.76, br s 23.2
19 0.89, d (6.6) 22.5
2′ - 170.2
3′ - 75.3
4′ - 110.3
5′ 3.44, dd (7.0, 4.1) 68.3
6′ a 3.86, dd (11.6, 4.1) 60.4
b 3.79, dd (11.6, 6.4)
7′ 2.86, s 29.5