Table 1.
No. | 1 | ||
---|---|---|---|
δH, mult (J in Hz) | δC | ||
1 | - | 213.2 | |
2 | - | 56.4 | |
3 | 2.32, d (10.0) | 54.8 | |
4 | - | 133.2 | |
5 | 5.25, br s | 128.0 | |
6 | 1.84, m | 37.7 | |
7 | eq | 1.82, m | 42.9 |
ax | 0.75, q (11.9) | ||
8 | 1.44, m | 33.5 | |
9 | eq | 1.71, m | 36.0 |
ax | 0.83, dq (2.7, 12.6) | ||
10 | eq | 1.29, dq (12.9, 3.0) | 25.8 |
ax | 1.02, m | ||
11 | 1.48, ddd (11.8, 10.5, 2.7) | 37.9 | |
12 | 0.88, s | 14.2 | |
13 | 2.67, dd (10.1, 3.4) | 57.0 | |
14 | 4.90, dt (9.3, 3.3) | 83.7 | |
15 | a | 2.70, dd (16.2, 3.1) | 50.3 |
b | 2.52, dd (16.2, 9.4) | ||
16 | - | 206.8 | |
17 | 2.09, s | 30.8 | |
18 | 1.76, br s | 23.2 | |
19 | 0.89, d (6.6) | 22.5 | |
2′ | - | 170.2 | |
3′ | - | 75.3 | |
4′ | - | 110.3 | |
5′ | 3.44, dd (7.0, 4.1) | 68.3 | |
6′ | a | 3.86, dd (11.6, 4.1) | 60.4 |
b | 3.79, dd (11.6, 6.4) | ||
7′ | 2.86, s | 29.5 |