Table 5.
Crystalline phases characteristic for the obtained defective TiO2-HIO3 samples.
| Sample | Crystalline Size and Phase Content | |||||
|---|---|---|---|---|---|---|
| Anatase | Rutile | Brookite | ||||
| Size (nm) | Phase Content (wt%) | Size (nm) | Phase Content (wt%) | Size (nm) | Phase Content (wt%) | |
| TBT | 5.97 ± 0.04 | 95.5 ± 1 | - | - | 6.1 ± 0.3 | 4.5 ± 0.9 |
| TBT-HIO3_0.5 | 6.09 ± 0.03 | 86 ± 1 | - | - | 5.50 ± 0.19 | 14 ± 1.5 |
| TBT-HIO3_5 | 5.43 ± 0.03 | 89 ± 0.5 | - | - | 5.2 ± 0.2 | 11 ± 1 |
| TBT-HIO3_20 | 5.14 ± 0.03 | 96 ± 1 | - | - | 4.0 ± 0.6 | 3.5 ± 0.5 |
| TBT-HIO3_50 | 5.70 ± 0.04 | 68 ± 3.5 | 9.08 ± 0.17 | 32 ± 17 | - | - |
| TBT-HIO3_75 | 5.67 ± 0.05 | 20.5 ± 3.5 | 6.57 ± 0.09 | 7± 1.8 | - | - |
| TBT-HIO3_100 | 6.3 ± 0.2 | 15 ± 3.5 | 7.45 ± 0.06 | 85 ± 1 | - | - |