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. 2020 Jun 16;9(6):787. doi: 10.3390/foods9060787

Table 3.

Date seed oil recovery based on extraction methods.

Method Conditions of Extraction Conclusions References
Soxhlet Extraction yield 5% (chloroform, hexane), 4 h
Extraction yield 1% (propanol, methanol), 4 h
The yield is better with non-polar solvents (n-hexane, chloroform) compared to polar solvents (methanol and propanol) Ali et al. (2015) [70]
Soxhlet Extraction yield 4.44%, hexane, 8 h The ultrasound- and microwave-assisted extractions reduced the extraction time compared to Soxhlet and of extraction yield compared to maceration Ben-Youssef et al. (2017) [71]
Ultrasound Extraction yield 6.18%, hexane, 15 g, 20 °C, 30 min
Microwave Extraction yield 4.74%, methyltetrahydrofuran (MeTHF), 15 g, 30 min
Maceration Extraction yield 4.04%, MeTHF, 15 g, RT, 30 min
Soxhlet Extraction yield 8.5%, hexane, 50 g, 78 °C, 3 h The extraction by ultrasound shortened extraction time when compared to Soxhlet, reduced energy consumption, and had higher yield. Jadhav et al. (2016) [72]
Maceration Extraction yield 4.2%, hexane, 50 g, RT, 3 days
Ultrasound Extraction yield 8.5% hexane, 50 g, 20 °C, 45 min
SC-CO2 Extraction yield 3%, 5 g, 40 min, 70 °C In this case, the oil yield was very low, probably due to several compatibilities of CO2 with the oil. Aris et al.
(2013) [73]
Soxhlet Oil yield 8.5%, 120 min, hexane The oil composition indicated the presence of low molecular weight saturated fatty acids. Ali et al. (2015)
[70]
Soxhlet Oil yield 9.78, 8, and 9.5%, methanol, ethanol and acetone, respectively The best conditions were found using methanol 15 °C above its boiling point, particle size range of 0.212–1 mm, 4 h. Al-Sumri et al. (2016) [74]
SC-CO2 Oil yield 14%, 250 bar, 333 K The pressure and the interaction between the pressure and temperature had a positive significant effect on the extraction yield Mehdi et al. (2019) [75]