Table 3.
Quantitative analysis of the secondary metabolites (PhytoScan) of the Clerodendrum volubile ethanol leaf extract (CVE) using gas chromatography-mass spectrometry.
| Pk# | RT | Area (%) | Library/ID ref# | CAS# | Quality |
|---|---|---|---|---|---|
| (1) | 3.601 | 2.16 | Glycine, N,N-dimethyl-, methyl ester | 8679 007148-06-3 | 86 |
| N,N-Dimethyl-3-methoxypropylamine | 8722 020650-07-1 | 80 | |||
| 2-Methyl-allyl ethyl ether | 1759 000557-31-3 | 50 | |||
| Dimethylaminomethyl-isopropyl-sulfide | 14996 077422-33-4 | 50 | |||
| (2) | 7.464 | 5.74 | Urea, triethyl-urea | 21278 019006-59-8 | 50 |
| (3) | 8.579 | 0.77 | 5-Hydroxymethylfurfural | 11338 000067-47-0 | 93 |
| 5-Hydroxymethylfurfural | 11339 000067-47-0 | 70 | |||
| 5-Hydroxymethylfurfural | 11337 000067-47-0 | 62 | |||
| (4) | 9.878 | 1.56 | 4-Acetylanisole | 25100 000100-06-1 | 94 |
| 3-Methoxyacetophenone | 25121 000586-37-8 | 76 | |||
| (5) | 10.895 | 1.77 | Benzoic acid | 26636 000100-09-4 | 96 |
| 4-Methoxy-benzoic acid | 26633 000100-09-4 | 95 | |||
| 4-Methoxy-benzoic acid 4-methoxy | 26632 000100-09-4 | 93 | |||
| (6) | 12.691 | 0.50 | Megastigmatrienone | 56052 038818-55-2 | 99 |
| 1H-1,5-Benzodiazepine, 2,3,4,5-tetrahydro-2,2,4-trimethyl-phenol | 56033 040358-38-1 | 70 | |||
| 2-(1,1-Dimethyl-2-propenyl)-3,6-dimethyl- | 56097 092617-73-7 | 62 | |||
| (7) | 13.113 | 5.13 | Ethyl-α-d-glucopyranoside | 72939 019467-01-7 | 74 |
| Ethyl-β-d-glucopyranoside | 60076 000709-50-2 | 53 | |||
| Methyl-β-d-arabinopyranoside | 35240 005328-63-2 | 50 | |||
| (8) | 13.528 | 2.18 | Methyl tetradecanoate | 104286 000124-10-7 | 74 |
| (9) | 13.684 | 0.95 | Germacyclopentane | 36709 004554-75-0 | 53 |
| (10) | 13.887 | 0.81 | Tetradecanoic acid | 91415 000544-63-8 | 97 |
| (11) | 14.089 | 1.36 | 6-Hydroxy-4,4,7α-trimethyl-5,6,7,7 α-tetrahydrobenzofuran-2(4H)-one | 61438 073410-02-3 | 93 |
| (12) | 14.268 | 1.32 | Guaifenesin | 62883 000093-14-1 | 72 |
| 2-Cyclohexen-1-one, 4-hydroxy-3,5,6-trimethyl-4-(3-oxo-1-butenyl) | 85356 077846-84-5 | 64 | |||
| (13) | 14.539 | 0.88 | Neophytadiene | 138502 000504-96-1 | 99 |
| Bicyclo[3.1.1]heptane | 17424 006876-13-7 | 55 | |||
| 2,6,6-Trimethyl-, (1.alpha.,2.beta.,5.alpha.)9-octadecyne | 111836 035365-59-4 | 53 | |||
| (14) | 14.747 | 0.67 | 9-Octadecen-1-ol | 128820 000143-28-2 | 70 |
| (Z)-6-Octen-1-ol, 3,7-dimethyl | 51056 000105-85-1 | 70 | |||
| Formate-6-octen-1-ol,3,7-dimethyl-, formate | 51061 000105-85-1 | 70 | |||
| (15) | 15.278 | 3.25 | Hexadecanoic acid, methyl ester | 130821 000112-39-0 | 98 |
| (16) | 15.636 | 5.39 | n-Hexadecanoic acid | 117419 000057-10-3 | 99 |
| (17) | 15.827 | 2.03 | Hexadecanoic acid, ethyl ester | 144309 000628-97-7 | 99 |
| (18) | 16.682 | 5.61 | 7-Octadecenoic acid, methyl ester | 155720 057396-98-2 | 99 |
| 9-Octadecenoic acid, methyl ester | 155758 001937-62-8 | 99 | |||
| (E)-9-Octadecenoic acid, methyl ester | 155754 001937-62-8 | 99 | |||
| (19) | 16.780 | 3.28 | Phytol | 155849 000150-86-7 | 98 |
| (20) | 17.046 | 9.02 | 9,12,15-Octadecatrienoic acid | 138418 000463-40-1 | 99 |
| (Z,Z,Z)-9,12,15-Octadecatrienoic acid | 138420 000463-40-1 | 99 | |||
| (Z,Z,Z)-9,12,15-Octadecatrienal | 123143 026537-71-3 | 91 | |||
| (21) | 17.196 | 4.08 | 9,12,15-Octadecatrienoic acid | 165643 001191-41-9 | 99 |
| (Z,Z,Z)-Ethyl 9,12,15-octadecatrienoate | 165627 1000336-77-4 | 99 | |||
| 9,12,15-Octadecatrienoic acid | 165642 001191-41-9 | 99 | |||
| (23) | 18.004 | 0.62 | Ethyl-9-hexadecenoate | 142080 054546-22-4 | 89 |
| Cyclopentadecanone, 2-hydroxy- | 102369 004727-18-8 | 70 | |||
| (24) | 19.575 | 0.54 | Hexadecanoic acid | 188252 023470-00-0 | 90 |
| 2-Hydroxy-1-(hydroxymethyl)ethyl ester | 188251 023470-00-0 | 87 | |||
| (25) | 19.824 | 1.19 | Phthalic acid, di(2-propylpentyl)ester | 233419 1000377-93-5 | 91 |
| Phthalic acid, di(oct-3-yl) ester | 233383 1000377-72-3 | 80 | |||
| Diisooctyl phthalate | 233361 000131-20-4 | 74 | |||
| (26) | 20.771 | 1.02 | n-Propyl 9,12,15-octadecatrienoate | 179097 1000336-79-4 | 93 |
| 7,10,13-Hexadecatrienoic acid, methyl ester | 124916 056554-30-4 | 91 | |||
| Methyl (Z)-5,11,14,17-eicosatetraenoate | 177257 059149-01-8 | 90 | |||
| (27) | 21.527 | 0.68 | Squalene | 243222 000111-02-4 | 99 |
| (28) | 22.832 | 0.55 | Gamma-tocopherol | 245804 007616-22-0 | 95 |
| (29) | 25.137 | 0.68 | 2-(4-Fluoro-phenyl)-4-(3-methyl-benzylidene)-4H-oxazol-5-one | 140918 1000296-71-2 | 55 |
| (30) | 25.801 | 0.52 | 4-Dehydroxy-N-(4,5-methylene dioxy-nitrobenzylidene) tyramine | 157264 1000111-66-9 | 53 |
Pk#: peak number, RT: retention time, area%: percentage area covered, library/ID ref#: library/identification number, and CAS#: chemical abstract scheme number.